(Part 1 of 2)

(Part 2 of 2)

(Part 1 of 2)

As extractors, we want maximum data about what we are extracting or distilling, and the Arometrix Extraction Finder and Fraction Finders provide that data in real time… during your run! Join us as we venture down the rabbit hole of spectroscopy, as applied to cannabis. 

We also talk to Fernando of Voodoo Extracts for real talk about California's cannabis black market. He takes us on a walk through the life of a traditional market producer, with first hand stories of paying off city officials and his headline-catching desert grow busts.

Last but not least, we catch up with Photon Noir, one of the pioneers that helped shape modern closed loop hydrocarbon extraction. Dylan is full of stories from the early days, and walks us through his work with FOAF on developing of the original 'Honey Pot' closed loop system.

Sheldon Lotspeich - Founder & CEO of Carbon Chemistry

Cameron Matin - Director Of Accounts at Infinite Chemical Analysis Labs

Neena Batth-Sihota - Founder & CEO of SanDayV

Radiant Hoang - Founder & CEO of Delta Munchies

Devon Miller - Founder & CEO of Hi On Nature

George Stantchev - CEO of Comerg

Karen Galas - CEO of Alchemy Extractors

Randy Reed - Co-Founder, Lehua Brands

Katie Urbano - Operations Manager, 3-Chi

Alexandra Harris - Host, CannaSci podcast / LA NORML

David Anthony Schroeder - Author, 7 Ways To Manage Pain With CBD

Dr. Bau Thai - Founder, Rapid Nerve Rescue

Steve Bonde - CTO, Boulder Creek Technologies

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to Episode nine of The Modern Extractor. This podcast focuses on the processes, equipment and science found in a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing, with each episode digging into a particular stage in that process. The shows are released in an order that follows the workflow through a lab as material makes its way from cultivar to concentrate. 

Jason Showard - 00:00:39 

Last week we had Jay Horton on the show. He's the founder of Genovations and the man that got me started distilling cannabis. We talked specific SOPs for wiped film and rolled film distillation. We went through how to push your machine to the absolute limit and get the maximum throughput out of a wiper. He hit us with a ton of distillation knowledge gained from his years of experience in the trenches cranking out liters, as well as his experience installing and training on Chemtech equipment. 

Jason Showard - 00:01:05 

Moving on to this week's show, let's catch back up with a work in progress. So far, we've performed a cold ethanol extraction in a centrifuge. We've cold filtered the resulting miscella through a lenticular filter. We ran the filtered miscella through a falling film evaporator to separate the oil and the ethanol. We decarboxylated the crude oil to convert the cannabinoids. We terp stripped, then we distilled the oil, creating some beautiful golden distillate. As I said last week, distillate is the end of the line for THC. 

Jason Showard - 00:01:34 

But today we'll take CBD distillate a step further in the purification process and crystallize it into 99.9% pure CBD isolate. Joining me on the show today is a man who has processed many a kilo of isolate. He's very well versed in the equipment, solvents and processes of CBD crystallization. He's usually found flying around the world installing and training on BR instrument crystallization reactors, as well as their patented spinning band distillation equipment. He certainly knows his way around a cannabis extraction laboratory. 

Jason Showard - 00:02:06 

Luke Van Trieste, welcome to The Modern Extractor. 

Luke Van Trieste - 00:02:09 

Hi, thanks for having me. 

Jason Showard - 00:02:10 

Absolutely. Where are you calling in from today? 

Luke Van Trieste - 00:02:13 

I live just outside Baltimore, Maryland. 

Jason Showard - 00:02:15 

Right on. You were telling me earlier it's a snowy day out there. It's a rainy day here in Los Angeles. 

Luke Van Trieste - 00:02:21 

Yeah, plenty of bad weather lately this winter. 

Jason Showard - 00:02:25 

So talk to me a little bit about your path to joining BR instruments. 

Luke Van Trieste -...]]>Luke Van Trieste of BR Instruments joins us to discuss CBD isolate crystallization. We get deep into the equipment, solvents, and SOPs used to crash out those crystals. We cover static and dynamic crystallization, as well as the continuous flow processes that are beginning to come online. In addition to the BR Instrument crystallization reactors, we discuss their patented spinning band distillation equipment.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to Episode nine of The Modern Extractor. This podcast focuses on the processes, equipment and science found in a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing, with each episode digging into a particular stage in that process. The shows are released in an order that follows the workflow through a lab as material makes its way from cultivar to concentrate. 

Jason Showard - 00:00:39 

Last week we had Jay Horton on the show. He's the founder of Genovations and the man that got me started distilling cannabis. We talked specific SOPs for wiped film and rolled film distillation. We went through how to push your machine to the absolute limit and get the maximum throughput out of a wiper. He hit us with a ton of distillation knowledge gained from his years of experience in the trenches cranking out liters, as well as his experience installing and training on Chemtech equipment. 

Jason Showard - 00:01:05 

Moving on to this week's show, let's catch back up with a work in progress. So far, we've performed a cold ethanol extraction in a centrifuge. We've cold filtered the resulting miscella through a lenticular filter. We ran the filtered miscella through a falling film evaporator to separate the oil and the ethanol. We decarboxylated the crude oil to convert the cannabinoids. We terp stripped, then we distilled the oil, creating some beautiful golden distillate. As I said last week, distillate is the end of the line for THC. 

Jason Showard - 00:01:34 

But today we'll take CBD distillate a step further in the purification process and crystallize it into 99.9% pure CBD isolate. Joining me on the show today is a man who has processed many a kilo of isolate. He's very well versed in the equipment, solvents and processes of CBD crystallization. He's usually found flying around the world installing and training on BR instrument crystallization reactors, as well as their patented spinning band distillation equipment. He certainly knows his way around a cannabis extraction laboratory. 

Jason Showard - 00:02:06 

Luke Van Trieste, welcome to The Modern Extractor. 

Luke Van Trieste - 00:02:09 

Hi, thanks for having me. 

Jason Showard - 00:02:10 

Absolutely. Where are you calling in from today? 

Luke Van Trieste - 00:02:13 

I live just outside Baltimore, Maryland. 

Jason Showard - 00:02:15 

Right on. You were telling me earlier it's a snowy day out there. It's a rainy day here in Los Angeles. 

Luke Van Trieste - 00:02:21 

Yeah, plenty of bad weather lately this winter. 

Jason Showard - 00:02:25 

So talk to me a little bit about your path to joining BR instruments. 

Luke Van Trieste - 00:02:31 

So this is actually my 10th year at BR Instrument. I basically started off in high school doing graphic design content and creating marketing materials. I worked there through most of high school and college, until I got my degree in chemistry. And then I transitioned into my role, into doing installations and trainings. So if you buy a piece of our equipment, there's a very good chance that I'll be the person that's actually there, you know, running you through the show. So, yeah, 10 years. It's exciting. 

Jason Showard - 00:03:08 

So give us a bird's eye view of BR instrument as a company. How'd its start? Where is it now? 

Luke Van Trieste - 00:03:14 

So we produce mostly spinning band distillation equipment, which is really useful for high purity applications or for difficult separations. So we see a lot of work in the petroleum, the pharmaceutical, environmental, analytical industries. And obviously, you know, cannabis and hemp has become a very big part of our company as well. So we really just, any kind of distillation is pretty much our wheelhouse. 

Jason Showard - 00:03:40 

All right. So are you guys primarily working right now in the cannabis and hemp industry or are you spread out amongst all of that currently? 

Luke Van Trieste - 00:03:50 

We're spread out amongst all of that currently. So we do a lot of international business as well, which probably represents about half of the total business for us. And at this point in time, at least, there's not a ton of cannabis and hemp, although it's starting to pick up around the world. But that may be another couple of years while other countries figure out, you know, imports and exports and stuff like that. 

Luke Van Trieste - 00:04:16 

So I'd say cannabis is about, domestic cannabis, is about half of it. And the international, that basically encompasses all the other things I mentioned. It's probably about the other half of it right now. 

Jason Showard - 00:04:28 

OK, I've been intrigued by your spinning band distillation for a while now. Last week on the show, we covered, actually the last couple of weeks on the show, we covered distillation of cannabinoids with a rolled film distillation unit. While this show is technically about CBD isolate and crystallization, I think while I've got you on the line here, it makes sense to go over spinning band a little bit. So tell me a little bit about spinning band. How does it work? 

Luke Van Trieste - 00:05:01 

So if you're familiar with the colloquial, short path distillation. So by that I mean a small flask with a short little column, and basically a very simple distillation model. And not in reference to a wiped film or a rolled film distillation with appropriate pressure. So like Lab Society or Summit or one of many other companies produce those short paths. It functions more similarly to that than a wiped film. 

Jason Showard - 00:05:33 

Yeah, I've on the show here previously. I've referred to those as a tabletop short path. While the rolled or the wiped film still technically a short path, I believe you're referring to the tabletop short path, correct? 

Luke Van Trieste - 00:05:45 

Correct. So basically we are a batch process where you're going to at the beginning of the run, fill up your flask with your starting material and then you're going to heat it up. And then by using different boiling points of the different compounds in there, we're going to slowly separate them out. And basically how we do that is, the way to separate a vapor from a liquid is to have them interact more. Strangely enough. And that's going to enrich both of those phases in their majority component. 

Luke Van Trieste - 00:06:19 

And so a spinning band. What we're doing is by highly agitating the column area, as vapors come off of the boiling flask that we've been heating, we're greatly agitating these vapors and making them slam into the liquid and along the wall of the column, and basically forcing tons of interactions with a very high refresh rate. 

Luke Van Trieste - 00:06:42 

And that gives you the highest purity out of fractional distillation. And so a comparable method would be, for like a tabletop short path, if you put in a packing substrate. And that basically gives you a surface area for the vapor liquid interaction. So a spinning band, it's a dynamic interaction where that surface is always being changed, it's constantly being refreshed. And there's definitely some other advantages too. Such as a spinning band is going to have generally a higher throughput for the purity that you get. Because as the cycle of boiling and condensing happens, the helix of the spinning bands pumps the rejected liquid that has been condensed back into the boiling flask to start the cycle over again. 

Luke Van Trieste - 00:07:32 

But vapors are basically able to travel relatively freely up the column because there's a large open space. It's just moving. So there's a couple of advantages. But purity is definitely the name of our game. 

Jason Showard - 00:07:48 

Yeah, I've basically from talking to you guys at the trade shows and reading on the Internet, the amount of theoretical plates that can be created with these is pretty impressive, but something that you really don't run into with a wiped or a rolled film unit. That would definitely be the upside. Now, I've heard some people in the industry say that a downside to a system like this or to your traditional short path is going to be something like residence time. What do you say to that? 

00:08:18  

I say that cannabinoids aren't as fragile as people like to make them out to be. I think that, you know, frequently people take maybe a little bit too much care. I think a lot of it has to do with the type of product that you're trying to make. I'd say that the maximum temperature is almost more important than your residence time. And basically the thought process behind that is a general rule of thumb for chemistry, is that by every 10 degrees Celsius you raise the temperature, you cause a reaction to happen twice as fast. 

Luke Van Trieste - 00:08:55 

So taking twice as long is effectively the same thing as doing something 10 degrees hotter, from a chemical reactions perspective. So I think, you know, if you're really concerned about residence time, I think maybe you should look at the maximum temperatures that you're incurring first instead. And as long as you're below 200, 190 Celsius, you're really not going to see a ton of stuff. 

Luke Van Trieste - 00:09:22 

The funky things start to happen at about 210 to 220 degrees Celsius, in my experience. That's where you'll start to see more and more rapid degradation. 

Jason Showard - 00:09:32 

OK, so with your style machine, also, the way that it functions, you're going to end up with the lighter stuff, which is typically more fragile, coming off first and getting out of there before the temperature rises anyway for the most part, right? 

Luke Van Trieste - 00:09:50 

Yeah, absolutely. We do a decent amount of terpene processing, too, as well. Which involves using virtually no heat and just vacuum. And so instead of heating something, we can just reduce the pressure which will cause us to distil over. And with terpenes, they tend to be quite low yielding, but for that very reason, you want to be very careful with them and very gentle with them. And those can be removed first in kind of a separate process, but still on the spinning band. 

Jason Showard - 00:10:18 

All right. Well, I'm glad we got a chance to kind of jump into that. I've wanted to talk to you guys about spinning band and had thought about reaching out regarding that. And then, you know, when it came up to reach out to you regarding crystallization, I figured it was a great opportunity to do that. So the reason that I reached out to you specifically about CBD crystallization is because of a blog post that you wrote back in early 2019 on the BR Instrument blog about creating CBD isolate. 

Jason Showard - 00:10:47 

It was full of equipment, knowledge and SOPs and just basically a really nice, informative package. In addition to the post afterwards, people started commenting and you were jumping right in there and responding to everybody's questions in the comments. I think that's great and really aligns with my approach here at The Modern Extractor, which is to kind of curate and release the best information possible to the audience. So because of that, I was excited to talk to you and I'd like to move on to the actual science behind the final stage in the process we've been covering this season, which is crystallization. 

Jason Showard - 00:11:20 

So let's talk a little bit about what we're trying to produce here. CBD isolate is purified, crystalized CBD. Let's break that down. So what is a crystal? 

Luke Van Trieste - 00:11:31 

So a basic overview of what a crystal is, is that it's going to be a solid that has its molecules in an organized long-range structure. And so I think it's important to talk about things that are not a crystal, so a very common example is a glass. Glass is clear, it's pretty. You can cut it into a crystal, but that doesn't make it structurally on the molecular level, a crystal. 

Luke Van Trieste - 00:11:58 

Another example is going to be like some kind of plastic or wax where, you know, these are very big molecules that kind of interact with each other in a much different way than a nice crystal lattice. I think it's also important to point out that a lot of natural substances are polycrystalline. And basically that's going to mean that you took a bunch of individual crystal structures, grew them together, and then they fused. So this is going to cover, you know, metals, some rocks or a ceramic, for example. 

Jason Showard - 00:12:30 

OK, so with those things that you were just talking about, for example, the metals, the rocks, the ceramic, that is, they were crystalline in nature prior to having a bunch of these crystalline structures formed together and then fused due to heat or some other environmental conditions? Pressure? 

Luke Van Trieste - 00:12:50 

Yes, you can almost think about the way they fused together as a joint. And so frequently that's where a weak spot in the crystal may form, is at the interface of two of these different sub crystals. And so you can call gold crystalline in some context, but you're not going to have a gold crystal, if that makes sense. It's going to be quite small, realistically. 

Jason Showard - 00:13:14 

OK, so solubility is an important concept when it comes to crystallization. Talk to us a little bit about the relationship between solubility and crystallization. 

Luke Van Trieste - 00:13:28 

So solubility is going to be in this case, how much CBD can we jam into a given solvent at a given temperature? And there's ways to change that. An important way is temperature. So as you increase the temperature of anything, it's going to become more soluble. And if you decrease the temperature, it's going to become less soluble. 

Luke Van Trieste - 00:13:54 

So we want to, our goal is to basically create a solution that has a lot of CBD in it and that's going to be called "saturated." So a saturated solution is when we get to the point where if you add more CBD, it doesn't dissolve anymore, it just kind of sinks to the bottom of the container. Then you can also have a supersaturated solution. 

Luke Van Trieste - 00:14:15 

So this is going to be a solution that has more CBD than it should technically be allowed to at that temperature. And how we create that is you elevate the temperature to dissolve a lot of CBD, but then through some controlled method, you reduce the temperature without crystalizing any of the CBD out of solution. Suddenly you have CBD that's just maybe a little bit thermodynamically unhappy to be there at this point, but it's not quite ready to crash out. 

Jason Showard - 00:14:44 

OK, well, before we get further down the road into the SOPs of crystallization and specific stuff about equipment, let's talk about solvents for a moment here. While you're talking about solvents, there's a variety of them that can be used for crystallization. Are you making solvent decisions based on solubility or is that more of a boiling point or regulation or a safety decision? 

Luke Van Trieste - 00:15:09 

So primarily the issue is solubility, because if it doesn't crash out at some point or you can't dissolve any of it, then that's just kind of a non-starter. So our solvent of choice really needs to have a couple characteristics regarding solubility. So the first one is that CBD needs to dissolve into our solvent well, at an elevated temperature like I mentioned. However, at decreased temperatures, when we start to cool our solution, CBD needs to become relatively insoluble. If it stays too soluble at a low temperature, then we're not going to get crystal formation. 

Luke Van Trieste - 00:15:49 

The final solubility consideration is what is our waste product consisting of? So if we have THC that needs to be removed from these CBD crystals so you can sell them internationally, then you need to make sure that your solvent of choice also carries THC quite well at low temperatures, not just high temperatures. Otherwise you're just going to end up with kind of a goo coating your crystals as it will crash out, but not really crystallize either. 

Jason Showard - 00:16:20 

Some CBD sauce. 

Luke Van Trieste - 00:16:22 

Yeah. So that's how you]]>6e18ce8d-c98b-47de-b4d7-5d547f5d1ca7Tue, 16 Feb 2021 05:00:00 -070057:44nofull19Jason ShowardS1 E08 - Devolatilization & Cannabinoid DistillationLook no further for DISTILLATION SOPs!

Jay Horton joins us to discuss getting maximum throughput and high quality distillates out of you wiped film distillation unit. We cover specific SOPs for terpenoid removal (terp strip) and cannabinoid distillation for both THC and CBD. We discuss getting maximum throughput on a single stage machine, as well as various ways to configure your multi stage distillation unit to maximize your results. Jay's 'split the stream' technique will get you the highest quality and largest quantity yields out of your multi-stage wiper.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:11 

Hello and welcome to Episode eight of The Modern Extractor. This podcast focuses on the processes, equipment and science found in a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through lab, as material makes its way from Cultivar to concentrate. 

Jason Showard - 00:00:37 

Last week we had John Hart, founder and CEO of Chemtech Services, on the show to talk about wiped film and rolled film distillation. He broke down what's going on inside of a wiped film distillation unit and helped make some sense of it. He hit us with a ton of distillation knowledge gained through his years of experience building high tech equipment for the chemical industry. Moving on to this week's show, let's catch back up with our work in progress. So far, we've performed a cold ethanol extraction in the centrifuge. 

Jason Showard - 00:01:03 

We've cold filtered the resulting miscella through a lenticular filter. We ran the filtered miscella through a falling film evaporator to separate the oil and the ethanol. And we decarboxylated the crude oil, converting the THC A or CBD A into THC or CBD. This week we're going to get into specific SOPs for removal of the terpenoids, also known as terp stripping, followed by distillation of THC and CBD. It's a big day today guys. We're finally going to make some sellable product. 

Jason Showard - 00:01:30 

Joining me on the show today is the man that got me started distilling cannabinoids. He's usually flying around the world installing and training on Chemtech's distillation equipment, or doing some type of cannabis lab consulting. He's the founder of Genovations and quite a veteran in the cannabis lab space. Jay Horton, welcome to The Modern Extractor. 

Jay Horton - 00:01:47 

Hello, Jason. 

Jason Showard - 00:01:48 

Where are you calling in from today? 

Jay Horton - 00:01:49 

I'm currently in Los Angeles. 

Jason Showard - 00:01:51 

All right. Yeah, I'm also here in Los Angeles, still hunkering down. So I met you years ago when you installed the first wiped film unit I ever worked with, at the company I was working for. It was a Chemtech Mini 5. By the time we were done, strapping upgrades to it, it was almost KD6. Since then, you started your own company, Genovations. Tell us a little bit about how you got into the field and what the path was like to starting your own business. 

Jay Horton - 00:02:20 

OK, so in around 2006, I moved to Oregon and got into the medical program and I was doing cultivation. In around 2013, I started working with the company that was looking into CO2 extraction very early on. We]]>Look no further for DISTILLATION SOPs!

Jay Horton joins us to discuss getting maximum throughput and high quality distillates out of you wiped film distillation unit. We cover specific SOPs for terpenoid removal (terp strip) and cannabinoid distillation for both THC and CBD. We discuss getting maximum throughput on a single stage machine, as well as various ways to configure your multi stage distillation unit to maximize your results. Jay's 'split the stream' technique will get you the highest quality and largest quantity yields out of your multi-stage wiper.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:11 

Hello and welcome to Episode eight of The Modern Extractor. This podcast focuses on the processes, equipment and science found in a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through lab, as material makes its way from Cultivar to concentrate. 

Jason Showard - 00:00:37 

Last week we had John Hart, founder and CEO of Chemtech Services, on the show to talk about wiped film and rolled film distillation. He broke down what's going on inside of a wiped film distillation unit and helped make some sense of it. He hit us with a ton of distillation knowledge gained through his years of experience building high tech equipment for the chemical industry. Moving on to this week's show, let's catch back up with our work in progress. So far, we've performed a cold ethanol extraction in the centrifuge. 

Jason Showard - 00:01:03 

We've cold filtered the resulting miscella through a lenticular filter. We ran the filtered miscella through a falling film evaporator to separate the oil and the ethanol. And we decarboxylated the crude oil, converting the THC A or CBD A into THC or CBD. This week we're going to get into specific SOPs for removal of the terpenoids, also known as terp stripping, followed by distillation of THC and CBD. It's a big day today guys. We're finally going to make some sellable product. 

Jason Showard - 00:01:30 

Joining me on the show today is the man that got me started distilling cannabinoids. He's usually flying around the world installing and training on Chemtech's distillation equipment, or doing some type of cannabis lab consulting. He's the founder of Genovations and quite a veteran in the cannabis lab space. Jay Horton, welcome to The Modern Extractor. 

Jay Horton - 00:01:47 

Hello, Jason. 

Jason Showard - 00:01:48 

Where are you calling in from today? 

Jay Horton - 00:01:49 

I'm currently in Los Angeles. 

Jason Showard - 00:01:51 

All right. Yeah, I'm also here in Los Angeles, still hunkering down. So I met you years ago when you installed the first wiped film unit I ever worked with, at the company I was working for. It was a Chemtech Mini 5. By the time we were done, strapping upgrades to it, it was almost KD6. Since then, you started your own company, Genovations. Tell us a little bit about how you got into the field and what the path was like to starting your own business. 

Jay Horton - 00:02:20 

OK, so in around 2006, I moved to Oregon and got into the medical program and I was doing cultivation. In around 2013, I started working with the company that was looking into CO2 extraction very early on. We went up to Washington to visit Fritz and checked out his systems, and it was some of the first ones he was making. And we did our research on waters as well, and we decided on getting a water system. So that's kind of where I transitioned from, cultivation into extraction. 

Jay Horton - 00:02:58 

From there, I moved to the Bay Area and started working with the company in Oakland doing CO2 extraction again, but on a different system. And that was my introduction to wiped film distillation as well. I started running a Chemtech that I had specked out after I did a bunch of research on different wiped film manufacturers. 

Jason Showard - 00:03:20 

So at what point did you decide, "Hey, I need a wiped film distillation unit?" 

Jay Horton - 00:03:26 

Well, I had done the research and at the time I had actually just using glass from Amazon, already distilled oil on a tabletop scale. And I didn't do much of that before I decided to start doing research to figure out how to not do much more of that. 

Jason Showard - 00:03:47 

Yeah, I feel you there. 

Jay Horton - 00:03:49 

Nothing against tabletops. And my setup was really crude because it was Amazon glass, and really tiny tubing and everything. There's cool stuff you can do on those tabletops in terms of isomerization and things. But nonetheless, I didn't want to do that because we were kind of more of a scale focused operation. So wiped film naturally was the route. I went up to Washington again to research equipment at Helderpad, I saw a demo and I told the company I was working for that was a system they should buy. 

Jay Horton - 00:04:22 

So I ran a Chemtech for a number of years. I was real hands on. Did all my own maintenance. And at one point Chemtech called me and they asked me if I could help a client who is nearby in the Bay Area. And so I went down there and I helped them out. They'd been working on days trying to figure out this problem. And I went down there and figured it out very quickly. And so then I called Chemtech and I asked them, "Hey, would you guys need any help in the field?" 

00:04:52  

And they said, "Sure, fly out here." So I flew out there. I got factory authorized and certified to work on their equipment. And so they contract me for their installs and the clients then end up contracting me for preventative maintenance and additional training and things of that sort. 

Jason Showard - 00:05:12 

All right. Right on. When was it that you decided, you know, hey, I want to get out of the lab and I want to start a business around doing this side of the world, doing installs and teaching people? 

Jay Horton - 00:05:25 

Yeah, it all started with that call from Chemtech when they asked me to go check out this client. And at that moment, I had the idea that maybe I could make a career out of just going from place to place, helping people with their systems. At that time, I didn't even think installs would be a thing. And I was really scared at the moment to leave my regular job and branch out, start traveling around. And I did that. 

Jay Horton - 00:05:52 

I took the leap of faith. And I'm really glad I did because I discovered that I like to teach people, and I really enjoy working with all the different people that I do all the time. It's kind of like the icing on the cake. 

Jason Showard - 00:06:07 

So if that's how it all began and got you started, what are you doing these days? 

Jay Horton - 00:06:13 

So I'm still doing installs for people. Still doing preventative maintenance for people. I'm doing training for people. I'm keeping busy moving used systems around because there's a lot of activity in that sector of the market right now, you know, used systems being sold. And I'm getting contracted to either do the disassembly or the reassembly or both. 

Jason Showard - 00:06:35 

OK, what companies do you currently work for? For your installation work? So primarily, Chemtech uses me as an independent contractor to do their installs. Then from there, the clients typically contract me themselves to do training or preventative maintenance programs with them. I've also helped Interchim with installations of their chromatography columns. Occasionally Interchim will contract us because of our experience with cannabinoids. 

Jason Showard - 00:07:06 

OK, well, you've been on the front lines of the whole cannabis reform thing for a while now. In your travels, you've seen first-hand how things have changed. What are some of the biggest differences that you see in these days compared to the early days? 

Jay Horton - 00:07:22 

I would say better practices in general compared to the early days, part of that's due to regulations, and part of it's also just because people are getting real investment now. So people are building GMP facilities and things of that nature, getting food certifications. 

Jay Horton - 00:07:40 

And people are getting organic certifications from third parties, not, unfortunately, FDA, but other ones or USDA, I should say. So that's, I'd say, the primary difference that I see. You know, back in the day when I first started doing the installs, I would install these systems in some places that just weren't really what you think of when you think of, like processing facility for medicine or food grade products. You know? 

Jason Showard - 00:08:14 

Certainly I've seen a few of them. 

Jay Horton - 00:08:17 

I'm sure you have. 

Jason Showard - 00:08:20 

So last week we talked to John Hart from Chemtech and we learned about how their rolled film distillation systems work. But this week I'd like to get a little more specific about the SOPs for cannabinoid distillation. Considering you're the person that started me down this path, I figure there's nobody better to talk to you than you about it. So let's get into how to turn the decarbed crude that we have so far in our process, into the distillate that we're looking for. 

Jason Showard - 00:08:50 

Right now, let's start with THC. And for the sake of simplicity, let's just say that we've got a one stage machine in front of us. One stage Chemtech rolled film machine. What are your go to SOPs when you walk up to a new batch of starting material? 

Jay Horton - 00:09:05 

OK, so typically in a perfect world, that batch is also going to come with a COA. And that COA is going to tell you what your terpene content is and what your cannabinoid content is. 

Jay Horton - 00:09:19 

If you don't have a COA, you're kind of flying blind. In general, I'd say a lot of ethanol extract has around 10% terpenes left in it after solvent recovery. It's kind of an average number. But, you know, butane or CO2 could have more. But we're talking about ethanol extract today and on average, that's 10%. But ideally, you actually have a COA to tell you exactly what percentage of terpenes by volume are left in your extract. So you actually know what to look for, and your ratio once you start distilling. 

Jay Horton - 00:09:52 

So that said, for a terpene strip. I typically will have my feed tank around 100 Celsius, my residue temperature around 130C. My evap temperature around 170C. My condenser around 35C. And the reason why I say around is because especially if you don't have a COA, and you're just flying blind based on consistency in your facility, then you will be relying a little bit on intuition and visual cues. Right. So you might bump up the evap a little bit. 

Jay Horton - 00:10:31 

Or if this material's residue wants to freeze, you might bump up your residues section. Vacuum wise, I'd like to stay in between about 500 to 1,500 micron. I'll go higher, I'll go up to 5,000 if I put some material in there. And it's just really volatile because there's a ton of terps left in it and I don't feel like running slow. Then I'll just bump up my evap and I'll push that upper limit. But usually I'm terp tripping 500 to 1,500 micron. And wiper speed, 400. 

Jason Showard - 00:11:07 

All right. Now when you say you're running fast, what kind of, what do you mean by fast? 

Jay Horton - 00:11:15 

So essentially what I do is, I have these vacuum ranges I like to stay within. And if I start feeding material and my vapor pressure hasn't bumped me up to my upper limit, then I'll continue to increase my feed and my evap so I could run faster. 

Jason Showard - 00:11:32 

Gotcha, gotcha. All right, your SOPs for 170 there are fairly on the, I'd say on the high range for most of the people that I talk to about terp strip. If you're going to go an evap temp of 170, at some point, you've got to be feeding pretty fast into that in order to not overdo it, right? 

Jay Horton - 00:11:59 

You're absolutely correct. It's all relative, it's about residence time. The faster that you can feed material through the call and the faster it pushes other oil through, so the less residence time it has on the heated surface. So although you may have a bath that tells you 170, that might not necessarily be the temperature that the oil gets to, depending on its residence time. Now, that said, the reason why I like to run hotter than most people will on a terpene strip is because from my observations. 

Jay Horton - 00:12:31 

Over the years, I've noticed that if you do an aggressive terpene strip, you can remove majority of terpenes and you might get a tiny bit of canna. This allows you to go into your cannabinoid pass and get 90% cannabinoids in a single pass.  

Jay Horton - 00:12:51 

Whereas people who don't go aggressive enough with their terp strip, typically have to do two cannabinoid passes in order to get the potency that the market kind of calls for now. 

Jason Showard - 00:13:03 

Yeah, absolutely. That's one of the things that when we were first getting started, you told me basically reach in there until you're pulling just a little bit of distillate over. And that way you're guaranteed that you've got the majority, or that you've got all of your terpenes out. Because you're already reaching in to that cannabinoid fraction. And then in addition to getting higher purity, your vacuum levels are so much better on your next pass when you're going through your distillate run. 

Jay Horton - 00:13:34 

Absolutely. And not only that, what a lot of people don't realize is that even in a short path distillation system, even on an aggressive terpene strip up to the point that you've pulled a little bit of cannabinoids, you probably still haven't removed, I can actually say almost guaranteed you haven't removed a 100% of the terpenes. Because then when you go to do your canna cut, and you have a hot condenser, which we'll get into later, any terpenes that are left in there will show up in your cold trap. 

Jay Horton - 00:14:02 

And on average I see 1% on the canna cut show up in the cold trap. So that just goes to show you that there's heavy terpenes in there that to reflux even in a short path. Which is one reason, side note, I prefer to terp strip on a short path with a lower vapor port specifically, and not on like a rolled film with an external condenser upper vapor port. Because those terpenes are that much more difficult to remove in a single pass. 

Jay Horton - 00:14:32 

And then you're putting more terpenes into your first canna cut, which should be your only canna cut ideally. And you're making it more difficult to achieve a potency on your first canna cut. 

Jason Showard - 00:14:44 

OK, let's talk a little bit about one of the things that people bring up to me when I start talking about reaching into that canna cut, just a little bit on your terp strip, is they don't want the loss. Now I came up with a little bit of a way to get that back. I'm curious to hear what yours is. What do you do when you've got some distillate in your terpene fraction that you have separated out? 

Jay Horton - 00:15:12 

OK, I'm really glad you asked that, because usually when I talk about an aggressive terp strip, people talk about that loss. Well, essentially, let's say that you do an aggressive terp strip to the point that you send those terpenes off for analysis. It comes back 20% canna in there, which is kind of high for an aggressive terp strip. That's still only 2% of the entire volume. And I'm not saying that you want to ignore 2% because you still don't lose it. 

Jay Horton - 00:15:40 

You simply shelf it, put it into living inventory. You can let time do the work for you if you want, or you could put it in a centrifuge to speed things up. And essentially the oil will drop out to the bottom. You could literally decant the terps just by simply pouring them off the top. You'll scoop out what's left in there, which is usually kind of sludgy because it's a combo of the canna with some of the heaviest terps. 

Jay Horton - 00:16:04 

And you could re-terp strip that and re-distil that. Now, at a rate like we discussed, let's just say high end, 20%. It's going to take a lot of those jars of terpene before you even have one jar of canna. And here's another very valid point. And you've talked about this before in the sense of biomass, where you kind of have to think about your efficiency. Right. In terms of grinding, in terms of everything. 

Jay Horton - 00:16:34 

Some people may be more efficient if they're able to do a single terp strip and a single canna pass and ignore that 2% until a rainy day. Then they can pull it back out and they can squeeze it for whatever they are, whatever they need to get out of it. Whatever they can get out of it. 

Jason Showard - 00:16:53 

Yeah, what I ended up doing was, I when we first talked about getting aggressive with the terp strip, I think I took that a little bit farther than you had intended for me to take that after]]>5df6e211-e31e-48e0-8a79-b38d6655e705Tue, 09 Feb 2021 07:00:00 -070050:48nofull18Jason ShowardS1 E07 - Wiped Film Evaporators For Cannabis Oil DistillationLearn how a wiped film evaporator works from the man that makes 'em best. John Hart, founder of Chemtech Services, joins us to discuss how his rolled film distillation machines are the best in the biz for the distillation of cannabis oil. John and Jason discuss the latest equipment offerings and innovations Chemtech is bringing to market, as well as the advantages to using multi-stage distillation units.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to Episode Seven of The Modern Extractor. This podcast focuses on the processes, equipment and science found inside a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through a lab, as material makes its way from cultivar to concentrate. 

Jason Showard - 00:00:39 

Last week we had Greg Arias of Concentrated Science and Aftermath Labs on the show. He helped us demystify decarboxylation on a molecular level. We talked a bit about the differences between decarbing THC versus CBD. And I talked through my decarb SOPs. Moving on to this week's show, let's catch back up with our material on its way through the lab. So far we've performed a cold ethanol extraction in a centrifuge. We cold filtered the resulting miscella through an insecure filter. 

Jason Showard - 00:01:06 

We ran that miscella through a falling film evaporator to separate the oil and the ethanol. And we decarboxylated the crude oil we separated, converting the acidic forms of the cannabinoids into THC or CBD. This week we make our way to the most complicated machine in the lab, the wiped film evaporator. Technically, we'll be talking about a rolled film evaporator today, which is the best style of wiped film for use in the cannabis sector. Joining us today to discuss rolled film distillation is John Hart, founder of Chemtech Services. 

Jason Showard - 00:01:35 

John and his team currently have a ton of equipment out there in the field. You'll find their machines installed at the premier cannabis processing laboratories throughout the country and all over the world. They're always working on developing new equipment for our industry and interesting R&D projects. But I'll let John tell you all about that. Without any further ado, John Hart, welcome to The Modern Extractor. 

John Hart - 00:01:54 

Oh, thank you very much, Jason. Happy to be participating. 

Jason Showard - 00:01:57 

Absolutely glad to have you on today. Where are you calling in from? 

John Hart - 00:02:01 

Calling in from our headquarters in Lockport, Illinois. Lockport's a suburb of Chicago. 

Jason Showard - 00:02:09 

Right on. All right. What's the weather like out there right now? 

John Hart - 00:02:12 

We have an amazingly sunny day here. Unfortunately, it's really cold. It's about 20 degrees Fahrenheit. 

Jason Showard - 00:02:20 

All right. I'm in Los Angeles now. It's got a little rain recently, but we could use it. All right. Anyway, what was your path like to starting Chemtech? 

John Hart - 00:02:32 

OK, so I'd spent most of my career working for a couple of major chemical companies, and I did a lot of things. I...]]>Learn how a wiped film evaporator works from the man that makes 'em best. John Hart, founder of Chemtech Services, joins us to discuss how his rolled film distillation machines are the best in the biz for the distillation of cannabis oil. John and Jason discuss the latest equipment offerings and innovations Chemtech is bringing to market, as well as the advantages to using multi-stage distillation units.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to Episode Seven of The Modern Extractor. This podcast focuses on the processes, equipment and science found inside a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through a lab, as material makes its way from cultivar to concentrate. 

Jason Showard - 00:00:39 

Last week we had Greg Arias of Concentrated Science and Aftermath Labs on the show. He helped us demystify decarboxylation on a molecular level. We talked a bit about the differences between decarbing THC versus CBD. And I talked through my decarb SOPs. Moving on to this week's show, let's catch back up with our material on its way through the lab. So far we've performed a cold ethanol extraction in a centrifuge. We cold filtered the resulting miscella through an insecure filter. 

Jason Showard - 00:01:06 

We ran that miscella through a falling film evaporator to separate the oil and the ethanol. And we decarboxylated the crude oil we separated, converting the acidic forms of the cannabinoids into THC or CBD. This week we make our way to the most complicated machine in the lab, the wiped film evaporator. Technically, we'll be talking about a rolled film evaporator today, which is the best style of wiped film for use in the cannabis sector. Joining us today to discuss rolled film distillation is John Hart, founder of Chemtech Services. 

Jason Showard - 00:01:35 

John and his team currently have a ton of equipment out there in the field. You'll find their machines installed at the premier cannabis processing laboratories throughout the country and all over the world. They're always working on developing new equipment for our industry and interesting R&D projects. But I'll let John tell you all about that. Without any further ado, John Hart, welcome to The Modern Extractor. 

John Hart - 00:01:54 

Oh, thank you very much, Jason. Happy to be participating. 

Jason Showard - 00:01:57 

Absolutely glad to have you on today. Where are you calling in from? 

John Hart - 00:02:01 

Calling in from our headquarters in Lockport, Illinois. Lockport's a suburb of Chicago. 

Jason Showard - 00:02:09 

Right on. All right. What's the weather like out there right now? 

John Hart - 00:02:12 

We have an amazingly sunny day here. Unfortunately, it's really cold. It's about 20 degrees Fahrenheit. 

Jason Showard - 00:02:20 

All right. I'm in Los Angeles now. It's got a little rain recently, but we could use it. All right. Anyway, what was your path like to starting Chemtech? 

John Hart - 00:02:32 

OK, so I'd spent most of my career working for a couple of major chemical companies, and I did a lot of things. I mean, I did mergers and acquisitions. I was an engineer on the technical side. So I was also building or let's say managing the construction of chemical plants in addition to chemical plants around the world. And I, you know, in the early part of my career, I spent about 60% of my time outside of the United States. 

John Hart - 00:03:00 

And the nature of my job was such that I actually earned some pretty significant dollars for the companies I was working for. So at some point in my career, I decided, gee, maybe I should just strike out on my own and see if I can earn a little more money myself than I was getting paid a salary. 

Jason Showard - 00:03:21 

At what point did you decide it was time to, you know, just go ahead and jump for it? 

John Hart - 00:03:26 

You know, I think I was about 50 years old. Maybe 51 or 52. But that's about the point in time I did that. And Chemtech has been around for 15 years, so that gives you a little bit of a time perspective. 

Jason Showard - 00:03:45 

So were you already in distillation when you were traveling around doing your other jobs? 

John Hart - 00:03:51 

You know, the chemical industry is such that the technologies I was working with did utilize distillation methods. And I mean, actually, my first major job at Ashland Chemical, Ashland was a subsidiary of Ashland Oil. So you can imagine distillation is a big part of processing oil. 

Jason Showard - 00:04:13 

Yeah, certainly is. So if that's how it all began, give us a little bit of a bird's eye view of what Chemtech is today. 

John Hart - 00:04:22 

OK, so I typically regard Chemtech as being two divisions. One division is the design and fabrication of our core technology, which is distillation systems. But we also do other technology, especially pilot plants for chemical companies, as may be required. The other division is our toll processing of chemicals division. And we have a lot of really major clients. I mean, I would say pretty much Fortune 200 companies. We distill some really sophisticated stuff. 

Jason Showard - 00:05:00 

OK, so what industries do you typically serve? 

John Hart - 00:05:04 

You know, historically we were very petroleum, petrochemical, specialty chemical oriented. In more recent years, obviously, the hemp and cannabis folks discovered that our high vacuum distillation equipment could be really useful for separating the cannabinoids from the other riff-raff molecules in the extracted oils. 

Jason Showard - 00:05:30 

I can certainly attest to that. I've used your machines and I absolutely love them. I'll get into what you offer in a moment here, but you've kind of brought up a great segway into the cannabis field. Tell me about the moment that you realized that your equipment was being used to distill cannabis oil. What was your initial reaction to that? 

John Hart - 00:05:50 

You know, it kind of started when a client out in California actually asked us if we could separate the CBD from a hemp oil that they were importing from Europe. And, you know, our reaction was, "Well, it's just another essential oil to us." And so we asked them to send us the sample. They sent us the sample. We processed it and sent the results back to them, the distillate residue fractions. And they were pretty happy because we had definitely separated and concentrated up the CBD. 

John Hart - 00:06:30 

So I think probably within about six months of that exercise, they bought a two-stage KD10 system from us, which they continue to operate out in the California area. Roughly about that same time, though, another California organization had called us and was asking for quotations on some of our smaller laboratory units. And we came to find out that they were distilling THC, and they ended up buying a lot of our lab scale units because they had multiple locations. Also about that time, we hooked up with an outfit called Helderpad, and Helderpad had a processing license in the state of Washington and they ultimately became our agent. 

John Hart - 00:07:21 

They were operating one of our units. They liked it and became our agent. They've done a really good job selling our equipment and they continue to distill out in their facilities in Seattle. 

Jason Showard - 00:07:33 

That's great. So a lot of the players in this space are making equipment specifically targeted at the cannabis market. Well, others kind of fall into the "fell into it" category because you already had something you made that was a good fit. From what you've explained to us so far, it seems like you are already in the game and then your equipment was just the right option for what the folks in the cannabis industry needed. With that said, what are you doing to keep the people that are targeting the cannabis field off your heels? Are you doing anything specific to stay relevant and hold your position? 

John Hart - 00:08:10 

Yeah, I mean, we actively have about six different R&D projects that actually are associated with more novel methods of processing cannabinoid molecules. But in the meantime, we've obviously embellished our existing offering to accommodate the industry. I mean, for example, we introduced some decarboxylation units into the industry a few years ago. We've also introduced specialty ethanol distillation units. Our two-stage distillation systems that will allow the user to get his ethanol content in the final oil down below a tenth of a percent. 

John Hart - 00:09:00 

And those obviously are peer reviewed. So they can pass the scrutiny of the regulators in the West Coast states. But like I said, we're continuing to work on things. I think one of the bigger novelties we brought to the industry also was the introduction of the turbo molecular pump into, not only cannabis processing, but short path distillation processing. Historically, the turbo molecular pump had been regarded as a little bit too fragile for distillation operations. But our primary supplier of vacuum equipment, Leybold Vacuum, came to us and said, "Hey, we have a new design. We'd like you guys to test it because we think it's robust enough to use in distillation." 

John Hart - 00:09:49 

So we actually engaged in a testing program that took longer than a year, and worked very closely with Leybold to develop the proper setup for the use of that turbo molecular pump in distillation. And I mean, just to give you an example, some of our early work was done with distilling epoxy resins, which are notoriously hard on the vacuum pumps. 

John Hart - 00:10:22 

But it turned out the pump ended up being pretty robust. And we introduced that into the industry. And absolutely, we're the first company to introduce the turbo molecular pump. And I think in general, the folks in the cannabis and hemp sectors like the turbo molecular pump. Like anything, any piece of vacuum equipment, it's got its pros and cons. But we're big fans of the turbo pump. 

Jason Showard - 00:10:48 

Yeah, I can certainly personally attest to the fact that you guys killed it on, you know, R&Ding that turbo. I had a counterpart I used to work with that we would be constantly doing battle about how hard to run things because I wanted to go easy on that turbo, and then I would leave for a couple of days and come back. And I know that it got tortured. So we actually went so far as to take the system apart and look in there, and you could see distillate built up on the blades of the turbo, which was killing me. But the thing just kept working. So well done on your R&D. 

John Hart - 00:11:23 

Yeah, no, it ended up being robust enough. I mean, we've also tried to get more focused on low temperature chillers and cold trap technologies to try and preclude the contaminants condensing into the turbo pump. 

Jason Showard - 00:11:42 

Yeah, that would be ideal. 

John Hart - 00:11:44 

Yeah. No, it is a constant battle. I mean the nature of the terpenoids in particular, they're good carrier molecules for some of the heavier or higher molecular weight molecules in oil extract. And these terpenoids are really tough to condense in the cold trap. You have to get to extremely low temperatures to achieve that. Maybe even as low as -100 degrees Celsius. But I mean, we went into it with knowledge that the folks who are using liquid nitrogen cold traps were tremendously successful in keeping their vacuum systems clean. 

John Hart - 00:12:26 

So we know if you get down to about -120 C, you're going to be running clean vacuuming equipment. 

Jason Showard - 00:12:35 

All right. That's good info. We'll jump into that in a little bit here when we get to the technical section. But you piqued my interest on a couple of things that you mentioned. Specifically your ethanol recovery and your decarb units that you've released for the ethanol recovery. Is that a system to recover all of the ethanol used in extraction, or is that specifically to get the residual ethanol out of your crude oil? 

John Hart - 00:13:00 

No, that's to recover the ethanol that's being used for ethanol extraction. 

Jason Showard - 00:13:07 

Okay, so all of it. 

John Hart - 00:13:08 

Yeah, all of it. All of it. And unlike many of our competitors, we are using a really, a fairly powerful vacuum pump on the system. You know, having said that, we typically like to see our clients run that system, maybe around 200 millimeters of mercury. Whereas that vacuum pump will easily take them down to one millimeters of mercury. 

John Hart - 00:13:31 

But at 200 millimeters, it operates pretty well. And when we designed the initial system, our target was 50 liters per our processing rate. And when we tested in our own facility, we saw that the system had so many features that were overkill that we were able to run the system at 200 liters per hour. So it's a robust system. 

Jason Showard - 00:13:58 

Wow, that is fantastic. If somebody wants to look that up on your website, what do you call that one? 

John Hart - 00:14:02 

It's a falling film/rolled film system, but it's probably indicated on the website under ethanol distillation. But it's a nifty little unit. I mean, "a little unit", it's being a two-stage unit, it's shall I say, bigger than most of the falling film and rising film units that you see out there. But like I said, the intent was to get that ethanol content to a low enough level that we could process the oil in our short path units. 

Jason Showard - 00:14:33 

So now from that stage, you mentioned decarb units. Do your units, is it a modular setup where you can put your decarb unit after this ethanol recovery unit? 

John Hart - 00:14:44 

Yeah, the decarb unit itself is a pretty independent unit with its own control enclosure. The only thing that I would caution anybody about, that's dealing with both ethanol, and let's say the de-ethylated oil, is ethanol, handling ethanol has to be done in a class one, division two electrical environment. Which, you know, is essentially an explosion proof environment. So the decarb unit itself is not really made in an explosion proof fashion. We can, but, you know, again, it's better to put your decarb unit and your short path unit outside of your classified zone. 

John Hart - 00:15:30 

And, you know, again, it's just a function of the equipment you use. For example, the turbo molecular pump, they don't make a class one, division two version of the turbo molecular pump. 

Jason Showard - 00:15:42 

Gotcha. Yeah. And it costs more money to build those C1D2 zones anyway. So if you can keep that as small as possible, you're going to end up building your lab in a more efficient manner. 

John Hart - 00:15:51 

Yeah, exactly. And if you've got open space, and you've got one space in that open space designated C1D2, then I think the, if I remember National Electric Code, if you get 15 feet beyond the classified zone, then you're outside the classified zone. So, you know, again, distance always helps when it comes to potential of flammable or explosive vapors. 

Jason Showard - 00:16:17 

All right. Interesting. What's the best selling item that you sell into the cannabis market specifically out of your offerings? 

John Hart - 00:16:25 

OK, so we sell a pretty broad spectrum of units. But if I had to pick any one unit, that seems to be a favorite, that would be the KD10 unit. Either in the single-stage or two-stage version. But the single-stage is a real workhorse. It's very easy to use. It's you know, everything is pretty much fully integrated into the skid, and we find our customers really like that unit. 

Jason Showard - 00:16:55 

All right. Yeah, I can agree with that one. I've seen them in use and had a chance to play with them. My original unit that I got from you guys was a Mini 5, that by the time we got done strapping extras on to it, it was almost KD6. And then I've had a chance to play with a friendly labs, KD10 for a little while. And that thing's a fantastic unit. It's beautiful. I love it. 

John Hart - 00:17:20 

Yeah. I mean, even our, the company that does most of our installs out in California, they look at the KD10 and they've told me it's a pleasure to install those units because they're so functional. 

Jason Showard - 00:17:35 

Getting a little bit more into the technical side of things here. I like to listen to podcasts kind of when my hands are full or I'm driving or riding a bike or just doing something where I can't watch video or look at pictures. And I think it's pretty common amongst most podcast listeners. So I try to cater to that audience....]]>a9c75933-aa22-48d2-b8cd-3587530907e2Tue, 02 Feb 2021 06:00:00 -070001:04:00nofull17Jason ShowardS1 E06 - Decarboxylation Of CannabinoidsLearn the ins and outs of decarboxylation from Greg Arias, co-founder of Concentrated Science. Greg and Jason discuss what is actually happening on a molecular level when decarbing your material, as well as specific SOPs for a streamlined and efficient decarb process.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to episode six of The Modern Extractor. This podcast focuses on the processes, equipment, and science found inside a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post-processing, with each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through a lab, as material makes its way from Cultivar to concentrate. 

Jason Showard - 00:00:39 

Last week on the show, we had Ray Van Lenten, founder and CEO of TruSteel on to help us break down falling film evaporation. Ray hooked us up with some amazing tips and tricks to get the most out of a falling film. He also broke down his decarb SOPs for use on their DR 10 decarboxylation unit. That's the same unit that I use and I absolutely love it. Moving on to this week's show, let's catch back up with our material on its way through the lab. 

Jason Showard - 00:01:06 

We've performed a cold ethanol extraction in a centrifuge and cold filtered it through a lenticular filter. Last week we took the resulting miscella and ran it through a Falling film evaporator to separate the oil we're after from the ethanol that we used to extract it. We were left with ethanol that's going to be sent back and used for future extractions and crude oil, which we're going to decarboxylate today. We heard Ray's decarb tech last week. But mine's a bit different. Let's get into it. 

Jason Showard - 00:01:33 

Now, I'd agree with Ray that a nitrogen sparge to push the air out of your decarb unit is ideal, but I've gotten pretty good results without doing it. Since, unlike Ray, I remove the solvent under vacuum. First off, fire up your cold trap chiller to protect your vacuum system. The condenser will catch any solvents removed from the crude. I like to bring my crude oil in and hold it at eighty degrees Celsius under vacuum of about -30 inches of mercury. 

Jason Showard - 00:01:57 

While it boils the remaining solvent off. It's important not to overfill the unit while doing this, or you can get some bumping of product into your condenser. This is a mess and it sucks to deal with, so don't overdo it. If you end up too full, you can lower your vacuum level a little bit. I bought the fourth ever DR 10 from TruSteel, so mine doesn't have an internal thermocouple to read the process temperature. I usually wait about fifteen minutes at 80C, then kick it up to 90 for about another ten minutes just to ensure all the solvent's gone. 

Jason Showard - 00:02:25 

Once I'm sure all the residual solvents are gone, I set my heater to 110C and start a timer for 40 minutes. Keep in mind that my process temp is 90 when I set that timer. Since I don't have an internal thermocouple, I don't have the ability to check the process temperature. So we just had to send out some lab tests along the way to make sure our decarb was going correctly. The oil makes it to 110 in, I would guess about ten minutes after I set it there, then spends another 30 at 110. 

Jason Showard - 00:02:54 

Then I immediately set the temperature on the heater back down to...]]>Learn the ins and outs of decarboxylation from Greg Arias, co-founder of Concentrated Science. Greg and Jason discuss what is actually happening on a molecular level when decarbing your material, as well as specific SOPs for a streamlined and efficient decarb process.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to episode six of The Modern Extractor. This podcast focuses on the processes, equipment, and science found inside a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post-processing, with each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through a lab, as material makes its way from Cultivar to concentrate. 

Jason Showard - 00:00:39 

Last week on the show, we had Ray Van Lenten, founder and CEO of TruSteel on to help us break down falling film evaporation. Ray hooked us up with some amazing tips and tricks to get the most out of a falling film. He also broke down his decarb SOPs for use on their DR 10 decarboxylation unit. That's the same unit that I use and I absolutely love it. Moving on to this week's show, let's catch back up with our material on its way through the lab. 

Jason Showard - 00:01:06 

We've performed a cold ethanol extraction in a centrifuge and cold filtered it through a lenticular filter. Last week we took the resulting miscella and ran it through a Falling film evaporator to separate the oil we're after from the ethanol that we used to extract it. We were left with ethanol that's going to be sent back and used for future extractions and crude oil, which we're going to decarboxylate today. We heard Ray's decarb tech last week. But mine's a bit different. Let's get into it. 

Jason Showard - 00:01:33 

Now, I'd agree with Ray that a nitrogen sparge to push the air out of your decarb unit is ideal, but I've gotten pretty good results without doing it. Since, unlike Ray, I remove the solvent under vacuum. First off, fire up your cold trap chiller to protect your vacuum system. The condenser will catch any solvents removed from the crude. I like to bring my crude oil in and hold it at eighty degrees Celsius under vacuum of about -30 inches of mercury. 

Jason Showard - 00:01:57 

While it boils the remaining solvent off. It's important not to overfill the unit while doing this, or you can get some bumping of product into your condenser. This is a mess and it sucks to deal with, so don't overdo it. If you end up too full, you can lower your vacuum level a little bit. I bought the fourth ever DR 10 from TruSteel, so mine doesn't have an internal thermocouple to read the process temperature. I usually wait about fifteen minutes at 80C, then kick it up to 90 for about another ten minutes just to ensure all the solvent's gone. 

Jason Showard - 00:02:25 

Once I'm sure all the residual solvents are gone, I set my heater to 110C and start a timer for 40 minutes. Keep in mind that my process temp is 90 when I set that timer. Since I don't have an internal thermocouple, I don't have the ability to check the process temperature. So we just had to send out some lab tests along the way to make sure our decarb was going correctly. The oil makes it to 110 in, I would guess about ten minutes after I set it there, then spends another 30 at 110. 

Jason Showard - 00:02:54 

Then I immediately set the temperature on the heater back down to 70. Again, I'm using an older DR 10, so I don't have the ability to cool my process down like the fancy new ones do. Once my heater reads an incoming temperature of 70, I'll drain the decarbed crude out of the system and send it on to the next stage in the process. Well, a lot of people talk about decarboxylation and everybody's got some decarb SOPs that they use. 

Jason Showard - 00:03:18 

Many don't understand the mysterious molecular magic that's actually going on inside your decarb vessel. And we're going to fix that. Joining us today to help break down decarboxylation, we have Greg Arias. Chemical engineer with Concentrated Science and Aftermath Laboratories. Greg is one of the smartest people I know and literally my first call as soon as I need to call in some science reinforcements. So without any further ado, Greg Arias, welcome to The Modern Extractor. 

Greg Arias - 00:03:44 

How's it going Jason? 

Jason Showard - 00:03:46 

Hey, pretty good man. Where are you calling in from today? 

Greg Arias - 00:03:49 

Calling in from my closet in Venice, California. That's the best place I could find to record around here. 

Jason Showard - 00:03:57 

I appreciate the little bit of extra care taken to make sure you sound good. Thank you. 

Greg Arias - 00:04:03 

No problem, man. 

Jason Showard - 00:04:05 

So Venice. You're a semi-recent transplant to the L.A. area in general. Tell us a little bit about your journey to working in the cannabis field here in Cali. 

Greg Arias - 00:04:18 

Yeah, of course. So back in 2013, I started my journey out west from New Mexico, my home state. Went to Arizona State University for my master's in chemical engineering, studied specifically fuel cell technology there. I was out in Arizona for about six years. I had always kind of wanted to come out to California anyway. That was my main goal. But I got a little side-tracked for about six years in my way, in Phoenix, I started distilling after I graduated. So I was making vodka, gin, rum, whiskey, you name it. All of the general spirits at Ohso Distillery. So - 

Jason Showard - 00:05:16 

That was fantastic, by the way. I was the beneficiary of some of those. They're great. 

Greg Arias - 00:05:21 

Appreciate that. Yeah. No, I had a lot of fun with that. That was a very, very cool little side quest, if you will, on the way out here. So, yeah, I was responsible for our recipe development, flavor creation, and things of that nature out there. So I was making all of the delicious spirits and flavors that people would be drinking on a daily basis out there. So during that time at the distillery, I had a friend turn me on to the cannabis industry. 

Greg Arias - 00:05:57 

She mentioned that one of her close friends was in a lab and looking for an assistant extractor because they were just taking off. Just like the industry seems to be doing right now. So I got in over there in 2017. Started doing some part-time work while I was still at the distillery. So I was in a supercritical carbon dioxide lab making extracts there. That was a short-lived little taste of the industry. That company was expansion of a larger Colorado company. They kind of phased themselves out after about two, three years there. 

Greg Arias - 00:06:52 

And, after that, I didn't really think about it much more until you called me up in January of 2019. 

Jason Showard - 00:07:04 

Glad I did too. 

Greg Arias - 00:07:06 

Yeah. Seriously, man. It was, you told me that there was some big opportunity out here in California to really get a taste of the industry, really start to build a career around it. And I had always thought when I was younger, I think it would be pretty cool to go into the cannabis research and development. Like actual lab scale proceedings of cannabis. But I never thought it would come to fruition as much as it did because of all the legislation out there. 

Jason Showard - 00:07:38 

Yeah, I remember when it was, I think it was Concentration 2019. We decided to meet up and have the conversation, and meet the team, and figure it all out. I'm very happy you made your way out. 

Greg Arias - 00:07:52 

Yes. And that was a fun weekend there at the Pala casino. I won't get into the details, but - 

Jason Showard - 00:08:00 

I think I'm still paying that off. 

Greg Arias - 00:08:02 

Yeah. Aren't we all? Why do they always have these conventions at casinos? I mean, is it. Well, we can make one guess as to why, but - 

Jason Showard - 00:08:13 

They know their audience well. 

Greg Arias - 00:08:15 

Yeah, of course. They know the risk tolerance of this audience. Right. 

Jason Showard - 00:08:20 

You got it. 

Greg Arias - 00:08:23 

So then after that. Moved out here. Started doing some terpene creation for a mutual friend of ours through Aftermath Labs, and we created our line of Sierra Turps and - 

Jason Showard - 00:08:44 

We'll shout out to Devon here. 

Greg Arias - 00:08:46 

Yep. Thanks a lot Devon. We appreciate it. 

Jason Showard - 00:08:49 

Yeah definitely. 

Greg Arias - 00:08:51 

Yeah, and then everything was going pretty good there as soon as I moved down. Then I think we all remember this very, in various capacities. But the vape crisis hit us. So that being the main outlet for the terpenes, that took a pretty big hit on the entire industry. So we kind of took a step back from there and - 

Jason Showard - 00:09:20 

Yeah, it came to a screeching halt and it was pretty brutal. 

Greg Arias - 00:09:22 

Oh, yeah. Now that was a tough time. And then wouldn't you know it right after that happened, then COVID hit. And then another couple of hits happened to the industry. So then that that led me to having to adapt, realizing that this was kind of the new normal now. Took a side career, so to speak, as I call it. As a sanitizer manufacturer. So I was a - 

Jason Showard - 00:09:52 

Yeah, I was right there with you, man. We jumped into that one together. 

Greg Arias - 00:09:56 

I remember. Yeah. Well, I don't think we'll ever forget that. That was a whole career in four months. A lifelong career in four months. It was unreal times. 

Jason Showard - 00:10:06 

That I was a wild story. Maybe we'll do a bonus episode on that ridiculoucity. 

Greg Arias - 00:10:10 

Yeah. That's a good idea. Spinoff. 

Jason Showard - 00:10:14 

Yeah. 

Greg Arias - 00:10:15 

And if anybody needs to know how to make good sanitizer, I've got a, I know a guy now. It's me so. Yeah. Then since then, after that kind of side quest if you will, into sanitizer, that's opened up a pretty large career of consulting for me. So now that I had had some cannabis knowledge under my belt, and now some sanitizer knowledge under my belt, I've been able to just kind of dance around doing some consulting for some labs up in Adelanto, California. And sanitizer consulting still down here in Los Angeles. Because that's just like the cannabis industry, I don't think the sanitizer industry is going anywhere anytime soon. 

Jason Showard - 00:11:09 

This is true. Just to clarify, for those of you who don't know Adelanto, it's one of the largest cannabis hubs here in Southern California. There's a ton of stuff going on down there. And I can attest to Greg doesn't want to toot his own horn here, but the lab that he's working at out there is fantastic. It is a facility, unlike anything I've ever seen before. It's awesome. 

Greg Arias - 00:11:33 

Looks like a P Diddy music video. 

Jason Showard - 00:11:36 

It really does. 

Greg Arias - 00:11:38 

It's well put together. It's very well thought out. And it is modern. It is very well-oiled machinery up there. And to just be a part of that is fabulous. Again, just to be at the forefront of, you know, modern technology in cannabis extraction is a very great gift, I think. 

Jason Showard - 00:12:01 

Yeah, yeah. And now you've kind of established a foothold here in town. You're tending to bounce around, a little less to just like whoever wants to hire you and more to whoever's got the hardest science and formulations that they're working on. I've definitely watched your schedule filled up over the past couple of years. And, you know, congratulations on that. What's the most interesting thing that you're working on currently or recently that you can talk about? 

Greg Arias - 00:12:26 

So not to get into too much detail. NDAs and proprietary information and whatnot. But cannabinoid conversions is the big one. Other than that, formulating is my main strong suit. Like you said, it's just trying to figure out what are the best recipes for making, for solving difficult questions that we have in the field. And this, of course, started when I was making terpene recipes here. But I'm most excited about my joint venture with you, Jason. 

Greg Arias - 00:13:04 

We're opening up a lab supply storefront, along with our general consulting services. So I'll be providing the lab-scale based consulting. So all of your analytical equipment, small scale research-oriented and development procedures. And then you, of course, will be doing the scale-up. 

Jason Showard - 00:13:31 

You got it, man. I couldn't have said it better myself. Definitely really excited about that one, too. It's been a long time coming. 

Greg Arias - 00:13:38 

Yeah, man. 

Jason Showard - 00:13:39 

I'll make sure to keep all you guys out there posted on the progress from that project as it comes along. Greg, circling back a little bit to what you mentioned prior to our side project. In regard to your solving difficult questions on the formulation work, I don't think I've ever seen you in a happier place than when you've got a hard problem on the desk in front of you. As far as formulation goes. It's definitely your sweet spot. Why do you think that is? 

Greg Arias - 00:14:05 

It's all a big puzzle out here. We're in one giant puzzle. There is methods to find it. There is language to find it. And that language is math and science, chemistry, physics. 

Jason Showard - 00:14:20 

Yeah. That's why I call you first man. 

Greg Arias - 00:14:22 

Yeah. 

Jason Showard - 00:14:23 

In regard to the conversions, something that I've heard you speak about a lot, which I find a really interesting analogy for it, is that you call it molecular Legos. Like you can basically take things apart, put them back together and really build from a molecular standpoint. I've always been more process-oriented. And like when I get you talking about the molecular Lego aspect, it's always fascinating to me. 

Greg Arias - 00:14:47 

Yeah, I kind of came up with well I'm not, I'm obviously not the first one because Legos are a thing before I was born. But I recall in undergrad, when I was studying organic chemistry under Dr. Yanser at New Mexico Tech. I'd first gotten my foray into developing novel anticancer drugs, and they would show me the skeletal structures of chemicals and, you know, kind of walk me through the process. This is the reagent that we add. This is the products that we get out and they look very similar. 

Greg Arias - 00:15:27 

And I'm like, "Oh, so you're just like putting pieces onto a smaller thing. Or taking off pieces. It's just like Legos. It's, and I love Legos growing up." So it's all like Legos that you can't see. You have to put it in a special machine to see, but it's Legos nonetheless. And that's just, it's just always has been fascinating, organic synthesis, organic decomposition it's just, it's wildly interesting to me. 

Jason Showard - 00:15:51 

It's a little bit tougher than building Legos, though, considering you've got to build Legos with a blindfold. And then finally, after you're done, take it off and see how you did. 

Greg Arias - 00:15:59 

Yeah, hope the best. Hope for the best yeah. It's kind of the magic of it, though right? Before photography became such a ubiquitous thing, you know, you would take a film photo and hope for the best. And that's kind of what it is. And that's, you're taking a little snapshot down here. And hopefully, it's what you want. And that's kind of like a pleasant surprise if you do get it. 

Jason Showard - 00:16:22 

Yeah, it's certainly some job security because there's a lot of people that are far less patient than you. 

Greg Arias - 00:16:28 

Oh man. It's just, you got to love what you do I guess. 

Jason Showard - 00:16:33 

That's true. So just the whole concept of not being able to see exactly what you're doing is a good segway into our main topic on the show today, which is decarboxylation. Up into this point of the process, you've really been able to get some pretty visual feedback about how you're doing. Decarb is one of the first stages where that's not necessarily the case. Well, it's definitely not the case. And in order to get feedback on that, you've got to really send it in for some lab...]]>c567c8b7-f39e-40f3-8db0-171f2ca262feTue, 26 Jan 2021 07:00:00 -070036:54nofull16Jason ShowardS1 E05 - Solvent Recovery In Cannabis ExtractionLearn the ins and outs of solvent recovery from Ray Van Lenten, founder and CTO of Trusteel. Trusteel's falling film evaporators completely revolutionized the solvent recovery game in 2018. Since then they've released an end to end suite of equipment to take you all the way through the extraction and distillation processes. Hear how Trusteel's gear can help break your lab's bottlenecks and streamline your operation. Ray gives us some awesome tips and tricks to speed you up on the falling film that definitely aren't in the owner's manual. Hear his SOPs for solvent recovery on the Autovap line, and his SOPs for decarboxylation in the DR-10. We've got times, temperatures, pressures, and feed rates on all the gear, and a special bonus at the end of the episode... METAL!

EPISODE TRANSCRIPT:

Jason Showard - 00:00:11 

Hello and welcome to episode five of The Modern Extractor. The podcast that focuses on the processes, equipment and science found inside a cannabis extraction laboratory. I'm your host, Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through a lab, as material makes its way from cultivar to concentrate. 

Jason Showard - 00:00:40 

Last week on The Modern Extractor, we had Maria Peterson on from Scott Laboratories to help us break down the intricacies of filtration. She's my go to filtration expert over at Scott. And with the help of her and Scott products, I've been able to get beautifully filtered extracts for years. Upon listening back to last week's show, it occurred to me that I really didn't mention Buechner filters and vacuum filtration. Probably because my brain somehow blocked it out as a defense mechanism. 

Jason Showard - 00:01:06 

But this is the way things were done for a long time. It's a very slow and miserable process where lots of things can go wrong. There's messes and broken filter papers and the list goes on. It's just not recommended for production scale. But for lab scale, it's not terrible to have one around for experiments. If you're using vacuum filtration or Buechner filters for production, Scott Labs' lenticular will absolutely change your life. Also, upon listening back, I realized that I didn't stress quite enough how important it is to filter while cold. 

Jason Showard - 00:01:35 

I've always tried to make sure that my miscella made its way through the filter before it had a chance to rise above -35 Celsius. Moving on to this week's show, let's catch back up with our material on its way through the lab. We've performed a cold ethanol extraction in a centrifuge, and cold filtered through a lenticular filter. This leaves us with a nicely filtered mix of cannabis oil dissolved in ethanol, which we refer to as tincture or miscella. 

Jason Showard - 00:01:59 

The next stage in the process is almost every extraction operations bottleneck, which is solvent recovery. One of our show's listeners, Tommy Ethanol, hit me up on Future4200 and said that I shouldn't skip over Rotary Evaporators and jump right into falling film evaporation. He's right. I shouldn't. I really wanted to, but I shouldn't. I think rotovaps for solvent recovery fall into a similar category in my mind, as the Buechner filtration I mentioned a few minutes ago. Something we'd all like to forget but are worth mentioning. 

Jason Showard - 00:02:26 

If anything, an understanding of the way things were for so long...]]>Learn the ins and outs of solvent recovery from Ray Van Lenten, founder and CTO of Trusteel. Trusteel's falling film evaporators completely revolutionized the solvent recovery game in 2018. Since then they've released an end to end suite of equipment to take you all the way through the extraction and distillation processes. Hear how Trusteel's gear can help break your lab's bottlenecks and streamline your operation. Ray gives us some awesome tips and tricks to speed you up on the falling film that definitely aren't in the owner's manual. Hear his SOPs for solvent recovery on the Autovap line, and his SOPs for decarboxylation in the DR-10. We've got times, temperatures, pressures, and feed rates on all the gear, and a special bonus at the end of the episode... METAL!

EPISODE TRANSCRIPT:

Jason Showard - 00:00:11 

Hello and welcome to episode five of The Modern Extractor. The podcast that focuses on the processes, equipment and science found inside a cannabis extraction laboratory. I'm your host, Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through a lab, as material makes its way from cultivar to concentrate. 

Jason Showard - 00:00:40 

Last week on The Modern Extractor, we had Maria Peterson on from Scott Laboratories to help us break down the intricacies of filtration. She's my go to filtration expert over at Scott. And with the help of her and Scott products, I've been able to get beautifully filtered extracts for years. Upon listening back to last week's show, it occurred to me that I really didn't mention Buechner filters and vacuum filtration. Probably because my brain somehow blocked it out as a defense mechanism. 

Jason Showard - 00:01:06 

But this is the way things were done for a long time. It's a very slow and miserable process where lots of things can go wrong. There's messes and broken filter papers and the list goes on. It's just not recommended for production scale. But for lab scale, it's not terrible to have one around for experiments. If you're using vacuum filtration or Buechner filters for production, Scott Labs' lenticular will absolutely change your life. Also, upon listening back, I realized that I didn't stress quite enough how important it is to filter while cold. 

Jason Showard - 00:01:35 

I've always tried to make sure that my miscella made its way through the filter before it had a chance to rise above -35 Celsius. Moving on to this week's show, let's catch back up with our material on its way through the lab. We've performed a cold ethanol extraction in a centrifuge, and cold filtered through a lenticular filter. This leaves us with a nicely filtered mix of cannabis oil dissolved in ethanol, which we refer to as tincture or miscella. 

Jason Showard - 00:01:59 

The next stage in the process is almost every extraction operations bottleneck, which is solvent recovery. One of our show's listeners, Tommy Ethanol, hit me up on Future4200 and said that I shouldn't skip over Rotary Evaporators and jump right into falling film evaporation. He's right. I shouldn't. I really wanted to, but I shouldn't. I think rotovaps for solvent recovery fall into a similar category in my mind, as the Buechner filtration I mentioned a few minutes ago. Something we'd all like to forget but are worth mentioning. 

Jason Showard - 00:02:26 

If anything, an understanding of the way things were for so long yesterday, makes us appreciate the way things are today a little bit more. It's worth noting here that it doesn't hurt to have a rotovap around the lab for other purposes. But a roto is definitely not where you want to be using for your primary means of solvent recovery. So let's break one down. A rotary evaporator or rotovap for short, is used to separate the cannabis oil from the solvent used to extract it. 

Jason Showard - 00:02:50 

The material that you'd like to separate is loaded into a glass round-bottom boiling or evaporation flask. The neck of that flask connects and seals to a motor assembly that will rotate it. The flask is held at about a 45 degree angle, with the liquid settling in the bottom side area of the round-bottom. The part of the machine that the flask is attached to, has the ability to be raised or lowered. Which allows for the bottom portion of the boiling flask to be lowered into a heated water bath. 

Jason Showard - 00:03:17 

The rotation causes the miscella inside to fully coat the interior of the flask, creating a thin film on all parts of the flask that aren't covered by the liquid. The liquid, thanks to gravity, constantly stays at the lowest point in the flask. Picture taking a stemless glass of wine, holding it at a 45 degree angle and rotating it. The bulk of the liquid always stays at the lowest point, but the rest of the glass is still coated in a thin layer and reapplied every time the glass passes under the liquid. 

Jason Showard - 00:03:44 

Vacuum is applied to the system. The motor is turned on to rotate the boiling flask and the spinning flask is lowered into the heated water bath. Under heat and vacuum, the ethanol is vaporized and the vapor's drawn towards the vacuum pump. Between the boiling flask and the vacuum pump, is a chilled condensing coil which re-condenses the vaporized ethanol back into a liquid state. The liquid runs down the condensing coil and drips into a collection flask ready to be used for future extraction. 

Jason Showard - 00:04:11 

As the ethanol is removed from the material in the boiling flask, the volume in the flask decreases and it becomes increasingly dark and viscous. The system vacuum can be utilized to suck more miscella into that boiling flask so the process can continue. This dance goes on until you find yourself with enough concentrated material in the boiling flask to warrant disassembling the machine and messily transferring the crude to another vessel. In addition to the slow recovery time, one other slight disadvantage to using rotovaps is the residence time your crude spends at temperature. 

Jason Showard - 00:04:42 

Since transferring out of the boiling flask is cumbersome, the concentrated crude keeps getting more miscella transferred in on top of it and remains at process temperature for extended periods. It isn't until you're done with a whole lot of evaporation, that you eventually dump out your freshly separated crude oil. The temperatures aren't high enough to do any real damage, but I think it's just generally good practice and procedure in the lab to expose your material to as little heat as possible while you're processing. 

Jason Showard - 00:05:07 

So there you have it, Tommy rotovaps not skipped. Hopefully now those of you that haven't had the pleasure of endlessly rotovaping have a better understanding of the solvent recovery landscape in 2018. Across the board, every extraction operation was hitting the same bottleneck of solvent recovery. Labs were just buying more and more rotovaps to have on the production floor. This resulted in more glassware to clean and possibly break. More operators to manage them all. It was a mess. 

Jason Showard - 00:05:33 

So today on the show, I'm very excited to speak to the man that solved the rotovap problem. He drastically changed the solvent recovery game. He's the first person to release a falling film evaporator to the cannabis market. He's the founder and CTO of TruSteel, Ray Van Lenten. Ray, welcome to The Modern Extractor. 

Ray Van Lenten - 00:05:50 

Thank you, Jason. How's it going? 

Jason Showard - 00:05:52 

Pretty good, man. Where are you calling in from today? 

Jason Showard - 00:05:54 

I'm calling in from my home recording studio here in Nevada City, California. 

Jason Showard - 00:05:59 

All right. I'm a little bit further south from you. Down in the Los Angeles area, trying to hunker down a bit and wait this thing out. So tell me a little bit about your humble beginnings. What did the path to starting TruSteel look like for you? 

Ray Van Lenten - 00:06:13 

About 2014-2013, is when I started my extraction journey. And I always found that the thing that I like to do more than actually processing, is scaling things up and finding new ways to do processes. So my chase towards perfecting the equipment and perfecting the process and trying to automate everything is kind of what ultimately led me to starting TruSteel. I'd been doing a lot of [inaudible 00:06:39] work and needed to build a falling film just out of necessity. And once I did build the first prototype, I realized that I really had something and maybe I should change my path in life and start TruSteel. And I'm really glad that I did. 

Jason Showard - 00:06:54 

Right on. What was it that brought you to decide you wanted to go the falling film route to recover your solvents? 

Ray Van Lenten - 00:07:02 

Well, I was running a rotovap. Do I need to say anything else? 

Jason Showard - 00:07:05 

Not to me, not at all. But as far as the listeners go, I mean, I'm sure plenty of people out there are familiar with the old taxing rotovap and it just crushes your time. But other than that, I mean, like, what was it that gave you the idea to decide, you know, "Hey, I'm going to build a falling film evaporator." Just looking at industry or what? 

Ray Van Lenten - 00:07:27 

Yeah. So obviously, you know, the bottleneck of the rotovap is what made me look at scaling it up. And really, I just got on Google and started looking up, you know, how do they recover solvent on a large scale. And first thing that popped up is a falling film evaporator. And I started looking at it as like, OK, you know, I think I could build one of these and put it together. So I had already had a decent supplier for a bunch of equipment that I already had custom made for my facility. 

Ray Van Lenten - 00:07:55 

And as anybody who's played with a tri clamp knows, it's fairly modular. So over time, I had ordered all the bits and pieces that I needed, and just kind of amassed them. Put it all together. And the first one just worked right out of the gate. I think it was like ten gallons an hour out of the very first prototype. 

Jason Showard - 00:08:14 

All right. Ready to throw your rotovaps out the window right there. 

Ray Van Lenten - 00:08:17 

Exactly. 

Jason Showard - 00:08:19 

Right on. So that's how it all began. Give us a current bird's eye view of TruSteel as a company. Where are you now? 

Ray Van Lenten - 00:08:25 

Yeah, so the first thing that we did is we scaled up our AutoVap line up. So we brought the AutoVap 30, which has full automation on it. Has a touch screen controller. And really, you set your parameters on it and all the operator needs to do is start and stop it. And then there's obviously a cleaning cycle once you're done. 

Ray Van Lenten - 00:08:44 

So our lineup now has an AV 15, a 30, 100 and a 300, and those numbers correspond to gallons per hour of ethanol recovery. So on top of our AutoVap lineup, there's obviously a bunch of other different pieces that you need to complete your lab. 

Ray Van Lenten - 00:09:04 

And one of our core values is having modular systems for processing, so that you can plug different devices in to create your ideal extraction chain. So, for example, we have a new product called the InstaCool. And its function is to cool down solvent completely inline. So instead of having a large vat that has a coil inside that you're hooking a chiller up to, and you're waiting hours for your solvent to come down. It has a series of heat exchangers on the inside in a pump, control screen, thermocouples, and a flow meter on the inside of it that essentially allow it to pump out of a storage tank, through the heat exchangers and cool down your solvent inline. 

Ray Van Lenten - 00:09:53 

And the idea is with the HMI and the PLC that we've put on the system, they can all talk to each other. And I'll use another example here, our Evo system, which is our wiped film evaporator. On the Evo, for example, your stage one, if you're having issues with vacuum, there's likely too much solvent, from your solvent recovery step. So the Evo can communicate with the AutoVap and tell it to slow down, so that it can strip out more solvent from your residue streams. So the idea is that all these little bits and pieces can kind of talk to each other and modulate to control your lab. 

Jason Showard - 00:10:33 

Wow, that's fantastic. You're going to put consultants out of a job, man. 

Ray Van Lenten - 00:10:38 

Yeah. And, you know, the idea is to have to different programmable recipes, and just kind of remove a lot of the human input. Just because humans make mistakes. And the nice thing is being able to data log, you know, and kind of have a receipt for whatever batch you have. 

Jason Showard - 00:10:53 

All right. So if that's what you guys got going on right now, what's the future look like for TruSteel? What do you see in the next year or two? 

Ray Van Lenten - 00:11:00 

We're hoping to put out a lot of full plants. So we've focused a lot of time on creating kind of all of the individual modules that you need. So now I think the focus this year is just putting it all together and making it all work as one giant facility. 

Jason Showard - 00:11:18 

With everything as crazy as it is right now with this whole pandemic or anything. Are you guys experiencing any kind of supply chain issues or anything like that? 

Ray Van Lenten - 00:11:28 

Previous to COVID, we've actually done a lot of work to bring a lot of our manufacturing sources back to the domestic market. So starting with our AV 30 and a majority of our lineup, at least 80 percent of our stuff is domestically sourced. And we were really lucky to do that in time before COVID because we're seeing a lot of shipping delays from China and some of these overseas companies. So that's done a really good thing for us. 

Ray Van Lenten - 00:11:57 

And another one of the things that COVID has kind of helped us bolster, is we weren't able to travel to the customer to install equipment. So we had to do a lot of documentation. And just kind of a lot of work to help guide some of our customers through the installs because we couldn't touch base. So it actually really strengthened our install team, and our project management teams' communications with the customers. And we were actually able to install two AV 30s in Colombia during the pandemic. 

Ray Van Lenten - 00:12:30 

And actually something really cool is our programmers speak Spanish as well. So our equipment is actually bilingual. So we were able to install equipment halfway across the world even during the pandemic. 

Jason Showard - 00:12:42 

That's fantastic. 

Ray Van Lenten - 00:12:43 

Yeah, I'm really proud of the team for doing that and just being able to handle it during this. So it's really made us stronger, if anything. 

Jason Showard - 00:12:52 

Yeah, so the AV 15 was basically the first falling film to market, it's really what put you guys on the map, or at least the first falling film into the extraction industry. Put you guys on the map. Shortly after that, you released the AV 30. 

Jason Showard - 00:13:07 

And just like, those machines completely changed the game for solvent recovery. I can speak to that myself after moving away from a rotovap into one of your AV 15s and it changed my world. So in previous episodes, we've talked about how you would use a falling film to separate the oil that you're after from the ethanol that you want to recollect. But let's get a little deeper into it. Give us a rundown of how your machines actually do that, like how do they work? 

Ray Van Lenten - 00:13:33 

So the entire machine is controlled by an Allen Bradley PLC system that's mounted outside of the hazardous zone. And the touch screen essentially takes all of the IO on the systems. So all the thermocouples and all the different inputs. Takes that and converts it to ethernet and allows it to talk to the PLC in a different room. So you can have all of your controls on the front of the system. But the actual PLC doesn't take up a lot of the room that you might see on some of these other systems, you know, that has a large panel mounted to the side of it. 

Ray Van Lenten - 00:14:04 

So it's nice to kind of be conscious about the space that you're taking up in your lab, for starters. But as far as the actual, the functionality of the system, you know, everything's controlled through the PLC. And the system has three pumps on it, there's a feed pump and then there's a residue and a distillate pump. I also like to use concentrate and condensate as distillate might be a little bit of a confusing term. Most people just think of THC distillate when in reality distillate is anything that you're distilling off. So it would be your condensate. 

Jason Showard - 00:14:37 

In this case, it would be your ethanol. 

Ray Van Lenten -...]]>62392096-f0f1-4e27-8b84-f01e07d38e00Tue, 19 Jan 2021 06:00:00 -070056:50nofull15Jason ShowardS1 E04 - Filtration Of Cannabis ExtractsCome on down the filtration rabbit hole! Jason discusses all things filtration with guest Maria Peterson of Scott Laboratories. Maria Explains why Scott Labs' lenticular filters are the best tool for the job when filtering your cannabis extracts. Also discussed are bag filtration, large scale cross flow filtration systems and how to build the ideal staged filter system to minimize your downtime and maximize your throughput.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to episode four of The Modern Extractor. This podcast focuses on the processes, equipment and science found inside a cannabis extraction laboratory. I'm your host, Jason Showard, and I work professionally in the cannabis extraction field. Here in season one. We're focusing on ethanol extraction and post-processing, with each episode digging deep into a particular stage in that process. The shows are released in an order that follows the progress of material through a lab as it makes its way from cultivar to concentrate. 

Jason Showard - 00:00:40 

First, let me take a minute to thank all the new listeners that have poured in over the last week. The show went from me being stoked every time I'd get a listener to, who are probably my friends that I sent links to, to absolutely blowing up over the last few days. Putting the show together is taking a lot of hard work and seeing the metrics go nuts makes it all 100 percent worthwhile. So very sincere and heartfelt thank you from me to all of you for tuning in. 

Jason Showard - 00:01:03 

Now, if I can talk you guys into subscribing and rating and reviewing the show, it'll help me book awesome guests for you in the future. Last week on the morning extractor, we had Adam Chambers on from Delta Separations to give us the latest from Delta. As a long-time processor prior to joining the Delta team, he gave us his go-to S.O.Ps for cold centrifugal extraction, as well as a ton of general extraction knowledge. This week takes us to the next stage, which is the filtration process. 

Jason Showard - 00:01:27 

Filtration is a difficult concept to wrap your head around. There's a lot of theorizing that goes on when you start to try to pick it apart. It certainly has a lot of feel to it, and it's hard to collect hard data about how and why things are happening. If you're the local filtration expert at your facility, that's certainly worth a feather in your cap. But if you're the filtration expert at the filter company, that makes you a complete boss in my book. 

Jason Showard - 00:01:48 

And that's exactly who we have with us today. Maria Peterson from Scott Laboratories is joining us on the show to discuss filtration. She's by far the most knowledgeable person I've ever spoken to on the subject. And I learned something new from her every time I get her on the phone. So without any further ado, Maria Peterson, welcome to the show. I'm really excited to have you on today. Tell us a little bit about your journey to becoming the filtration expert at Scott Laboratories. 

Maria Peterson - 00:02:10 

I was a winemaker for ten, I think about ten years. All over the world and kind of floated from one hemisphere to the next to be able to do two harvests in the same year and get as much experience as I could. Because, you know, you can go to university and get a degree in something. But then once you leave, you really quickly find out that, you know nothing. 

Maria Peterson - 00:02:38 

You know very little about the practicalities of making wine and getting something into a bottle, you know. That]]>Come on down the filtration rabbit hole! Jason discusses all things filtration with guest Maria Peterson of Scott Laboratories. Maria Explains why Scott Labs' lenticular filters are the best tool for the job when filtering your cannabis extracts. Also discussed are bag filtration, large scale cross flow filtration systems and how to build the ideal staged filter system to minimize your downtime and maximize your throughput.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to episode four of The Modern Extractor. This podcast focuses on the processes, equipment and science found inside a cannabis extraction laboratory. I'm your host, Jason Showard, and I work professionally in the cannabis extraction field. Here in season one. We're focusing on ethanol extraction and post-processing, with each episode digging deep into a particular stage in that process. The shows are released in an order that follows the progress of material through a lab as it makes its way from cultivar to concentrate. 

Jason Showard - 00:00:40 

First, let me take a minute to thank all the new listeners that have poured in over the last week. The show went from me being stoked every time I'd get a listener to, who are probably my friends that I sent links to, to absolutely blowing up over the last few days. Putting the show together is taking a lot of hard work and seeing the metrics go nuts makes it all 100 percent worthwhile. So very sincere and heartfelt thank you from me to all of you for tuning in. 

Jason Showard - 00:01:03 

Now, if I can talk you guys into subscribing and rating and reviewing the show, it'll help me book awesome guests for you in the future. Last week on the morning extractor, we had Adam Chambers on from Delta Separations to give us the latest from Delta. As a long-time processor prior to joining the Delta team, he gave us his go-to S.O.Ps for cold centrifugal extraction, as well as a ton of general extraction knowledge. This week takes us to the next stage, which is the filtration process. 

Jason Showard - 00:01:27 

Filtration is a difficult concept to wrap your head around. There's a lot of theorizing that goes on when you start to try to pick it apart. It certainly has a lot of feel to it, and it's hard to collect hard data about how and why things are happening. If you're the local filtration expert at your facility, that's certainly worth a feather in your cap. But if you're the filtration expert at the filter company, that makes you a complete boss in my book. 

Jason Showard - 00:01:48 

And that's exactly who we have with us today. Maria Peterson from Scott Laboratories is joining us on the show to discuss filtration. She's by far the most knowledgeable person I've ever spoken to on the subject. And I learned something new from her every time I get her on the phone. So without any further ado, Maria Peterson, welcome to the show. I'm really excited to have you on today. Tell us a little bit about your journey to becoming the filtration expert at Scott Laboratories. 

Maria Peterson - 00:02:10 

I was a winemaker for ten, I think about ten years. All over the world and kind of floated from one hemisphere to the next to be able to do two harvests in the same year and get as much experience as I could. Because, you know, you can go to university and get a degree in something. But then once you leave, you really quickly find out that, you know nothing. 

Maria Peterson - 00:02:38 

You know very little about the practicalities of making wine and getting something into a bottle, you know. That is that is quite the thing. So then my journey eventually led me to the US, and I met the folks at Scott Labs. And, you know, the conversation started like, "We need this person that can talk to other customers about filtration." And I'm like, "Oh, good luck. That's a gray area where you can pretty much get lost." Because the thing about filtration is that it's designed to make you feel insecure. If you don't feel a little bit insecure about it, there's probably something wrong with you if it doesn't maybe challenge you every now and then. 

Jason Showard - 00:03:30 

Yeah, yeah. It was those challenges that actually ended up having me get you on the phone for the first time. 

Maria Peterson - 00:03:36 

Oh, good. 

Jason Showard - 00:03:37 

Call in with enough nerdy questions and you eventually get escalated up to top tier support, which is Maria and team. 

Maria Peterson - 00:03:45 

Oh my goodness. Yeah. That's what happens, is nobody else will take the call. They're like, they don't want to say, "We just don't know." You know, that's what I really like about the team at Scott Labs that they're always looking to learn and to figure it out and to not tell the customer, "Hey, man, sorry, you're on your own." It's going to be either, "We'll get back to you on this one. We have to kind of ask some people, because I certainly don't have all the answers, but I know a lot of much smarter people than I to get me those answers." And then kind of because they're such smart people, it translated to normal people such as you and I. 

Jason Showard - 00:04:26 

Yeah, it's had to have been kind of an interesting path for you jumping into this new market with a whole new set of challenges that are not the same challenges that you find in the wine industry. 

Maria Peterson - 00:04:38 

Definitely, it keeps it interesting and keeps you thinking on your feet and kind of looking at, you know, the same old thing that you may have sold to a winemaker or a brewer and going, "Oh, wait, wait a minute. This is not for, this is not the way. They're not going to be fermenting something." So now we're not necessarily dealing with things like yeast and bacteria. Now we're looking at all those lovely colloidal materials like lipids and waxes and things that like to show up when you chill them, for example. 

Jason Showard - 00:05:18 

Yeah, exactly. So some of the players that are in the extraction space are there because they really went after it and targeted it, and others kind of have fallen into it. I'd imagine already being established in the beverage space. You guys fall into the "fell into that" category. Tell me what some of the conversations were like when you guys realized over there that you had a whole new group of customers. 

Maria Peterson - 00:05:46 

Well, it was like, "Oh, wow, these guys." It was like I was excited because, you know, having worked in the wine industry on the East Coast, it was and in the Bible Belt, that it was always, you know, alcohol in many of the parts in the southeast is still a no-no. 

Maria Peterson - 00:06:07 

And it was and, you know, you have to go back to church if they found you drinking, for example. So I was always preaching like, "No man. Prohibition has been over for like 80 years. It's time. It's time to, like, let go of those beliefs." And all of a sudden in California, I found myself talking to people from all over the country that just had this, you know, it felt like they were finally allowed to have the conversation and not feel like you're in danger of somebody listening in and being like, "You're going to jail for having cannabis." You know, kind of thing. 

Maria Peterson - 00:06:48 

So I found it really refreshing. And then the people that, the people in your space, they are mostly extremely knowledgeable about extraction and can spin lovely biochemistry stories about things that that just makes me marvel. And I think it's fantastic. 

Jason Showard - 00:07:11 

It's a really great group of people with a good energy of exploration. And they're all used to wearing a lot of hats. Because for so long you really couldn't make the phone calls to ask questions. So I think a lot of the people that they gravitate towards this field, are people that are good at wearing a lot of hats and good at figuring things out, or have a really great group of friends that they can ask questions of. But for the most part, I think really, it's just people that are the jack of all trades that is going to be able to make it happen. 

Maria Peterson - 00:07:43 

Right. 

Jason Showard - 00:07:43 

That said, it's like it's a fun group of people to hang out with and to interact with and to problem solve with because they're skilled at it. 

Maria Peterson - 00:07:52 

Definitely. I find that most of the calls I get is from really open-minded people that can think laterally. And they normally, which is a funny one, is they would call and say, you know, "This is what I'm looking for. This is how I'm going to do it." They already have an idea of what they want. The ones that don't are like, "What are the other folks doing?" And it's kind of like, "This is the middle road. You know, this is kind of what most people are doing." But some of the others are very, they're very sure of what they want. And they would very rarely call back to say something didn't go well. And this is something where winemakers, ah, poor winemakers. I have to kind of talk behind their back a little bit, but they will call immediately and say, "How did this go wrong? I can't make this mistake again because it's not working. Help me figure it out." And with the like, I call you guys the botanical extract community. 

Jason Showard - 00:08:58 

Yeah, yeah. I learned real quick that that was the code word I had to use when I called in if I wanted to talk to anybody over there. 

Maria Peterson - 00:09:04 

Oh, my gosh, that's crazy. 

Jason Showard - 00:09:06 

If you didn't say botanical extracts and you said cannabis, we got shoved off to another vendor. 

Maria Peterson - 00:09:12 

So I and I don't want to make the people that are extracting peppermint oil feel bad about not having CBD and THC in their setup, you know. 

Jason Showard - 00:09:22 

So it really is botanicals. 

Maria Peterson - 00:09:24 

Exactly. And so and so, yeah, they would say, "This is what we want." And you guys really call back and say, "This didn't go so well." And the feedback is always appreciated because we don't learn if we don't hear back. But on the other hand, I'm always also very grateful not to hear back because I assume no news is good news. 

Jason Showard - 00:09:51 

Exactly. Yeah, the IP in the cannabis industry is very protected. Everybody kind of holds everything they're doing close to their chest. So I'd imagine walking into a winery, it's an older craft and a lot of the tricks of the trade are already kind of out there. So it'd be easier to get straight answers about, you know, what they're doing and then figure out how you can help them. 

Maria Peterson - 00:10:12 

Oh, sure. 

Jason Showard - 00:10:13 

But there may be a little bit of resistance in the sharing of information in our field I'd imagine. 

Maria Peterson - 00:10:19 

Yeah, yeah. It's and it's really, you know, my goal when I talk to someone is really to try and figure out how can we make your life easier in the long term. We're not just looking at how is next week going to go, but we're looking at, if it's something like as simple as a flow rate or a batch size. How is it looking now? And then if you were to dream, or you were to project, would that change? And if it changes, how would it change? 

Jason Showard - 00:10:50 

All right, so circling back a little bit to the fact that Scott kind of fell into the extraction space because they already had a great product that also worked for ethanol extraction. Now that the lenticular filter's kind of become an industry standard. There are some people that are directly marketing filters to the extraction space and really nipping at your heels. What are you guys doing as a company to hold your ground there? Are you marketing any products directly to the extraction space or making any product design decisions that are extraction focused? 

Maria Peterson - 00:11:32 

Right. Very good question because it's a little bit about supply and demand. And it's a tough one, because if the majority of the industry says, "We want a one-micron lenticular module." But you chill something down and you bring a number of colloidal materials and components out of solution, is it the most efficient to go so tight so quickly, or would it be more efficient to go slightly coarser and get a better throughput? And so if the industry comes with you and says, "No, no, no, we want a one-micron, because this is what the company that sells our extraction equipment uses and we just want to do what they do." Then having the conversation is kind of like it's better to wait until the student is ready for the teacher to appear so that when they run into, it's time to be more efficient, how can we use, how can we get more out of our filter media? 

Maria Peterson - 00:12:38 

Then you can say, "Oh, well, let's look at what are you trying to remove? These are the efficiencies." Then, there's a lot more questions coming up. So it's two-pronged. It's being there when the industry says, "This is what we want, and we've already decided about this." And then after a while when there's already been a little bit of this going on, then you can say, "Oh, well, if you want to be able to remove more of these components consistently, maybe let's try another grade and see how that goes. And let's take notes and see if that is even relevant." 

Jason Showard - 00:13:21 

OK, that makes sense. What would you say that your most common product sold into the extraction space is? 

Jason Showard - 00:13:28 

So typically this is how the majority of our customers would go. They would, depending on their extraction equipment, they would or would not need an extra something like a bag filter housing or a screen just to pick up rogue plant material that might have come through. And then you would go. Then you want dirt holding capacity like. So if you, if we look at the term dirt holding capacity, we're looking at kind of a media that has a lot of, let's call it a labyrinth. 

Maria Peterson - 00:14:06 

Right. So it's like a tortuous path that these, that the liquid has to go through for all these particles to be caught. And the reason why lenticular media is so popular is because it's a cellulose-based media that carries a charge. So you have a three-pronged method of retention. You have surface filtration. So whatever gets stuck on the surface will then build up a layer. And as that layer, whether it's visual or visible to the naked eye or not, that will keep on building up as the filtration progresses and that builds more surface area as you go. 

Jason Showard - 00:14:48 

Yeah, your filter quality ends up being a better-quality filtration towards the tail end of that media. 

Maria Peterson - 00:14:54 

Exactly. 

Jason Showard - 00:14:55 

But man does it take a lot longer? 

Maria Peterson - 00:14:57 

Right, exactly. And then you have charge in this media. You know, if there is a filter aid in that media like diatomaceous earth or perlite or resin. Those all contribute to charge that will then hold on to a counter charge. So that's the second mode. And you don't have that kind of charge with things like a bag filter, which is normally polypropylene felt. That's not going to hold onto things that have a charge unless they're big enough a particle to just not get through. 

Maria Peterson - 00:15:33 

But most colloids are like so squishy and soluble, they can get where they need to be if there is no charge. And then you have just really that tortuous path that's just holding onto particles because literally they can't get through. So that's why lenticular in particular is so good because you have the same charge that you would on a filter sheet. But it's in this modular form, which is a closed system. So there are a bunch of advantages to it. And we'll probably get into that a little bit, in a little bit. 

Jason Showard - 00:16:13 

Yeah, exactly. We'll jump into the technicals here in a minute. But I think I just learned something from you. Are you saying that the actual colloidal materials are being caught by the charge? More so than the actual filter mesh size? Is that accurate? 

Maria Peterson - 00:16:33 

That is exactly accurate. So it really is fascinating. If you look at diatomaceous earth in particular, you've got these fossilized algae, is really what it is, and it is mined. So that sounds all very like cloak and dagger, right, if you think about it. It's like hey we're using historical material to filter this, but it's still one of the most efficient ways to break charge. And you get diatomaceous earth and use for all kinds of things in different grades. 

Maria Peterson - 00:17:11 

So the grades that are used in making filter media is some of the purest. It's a very small amount that's normally used in this kind of filter media, but with lenticular specifically, it's the same media as filter sheets, but it's just put in this modular form. 

Jason Showard - 00:17:30 

All right, that's some good information. Let's jump around a little bit and we'll get into the technicals of lenticular filter before we get too techie on how exactly it works. Can you give us a rundown of what a lenticular is, what it looks like? We can get into the bell housing and...]]>4913cedf-c047-4619-b4bf-d009ee71b4d7Tue, 12 Jan 2021 00:00:00 -070057:49nofull14Jason ShowardS1 E03 - Centrifugal Extraction Of CannabisLearn the tricks of the trade for centrifugal ethanol extraction. Jason talks to Adam Chambers of Delta Separations about how their CUP line of ethanol extractors are the best tool for extracting the most out of your biomass, as well as all the other equipment offerings Delta has released recently. Times, temperatures, and SOPs that Delta usually charges for training on are 'extracted' in this interview.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:11 

Hello and welcome to Episode three of The Modern Extractor, the podcast that focuses on the processes, equipment and science found in a cannabis extraction laboratory. I'm your host, Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post-processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the progress of material through a lab, following it from Cultivar to concentrate. 

Jason Showard - 00:00:39 

Last week we discussed how to select quality biomass to extract from. After listening back to the show, I feel like I said a lot about what could go wrong there and neglected to mention that forming great relationships with your local growers is the absolute best way to consistently get quality biomass. In the second half of last week's show, we talked to Bri Tolp from Futurola about how their shredders can get you to your ideal mill sites for extraction. It was a great show and definitely worth a listen if you haven't already. 

Jason Showard - 00:01:08 

This week takes us to the next stage, which is the extraction process. We've got Adam Chambers from Delta Separations on today to give us the latest from Delta, as well as breakdown how their revolutionary CUP Series centrifuges will get you the most out of your material. So without any further ado, Adam Chambers, welcome to The Modern Extractor. 

Adam Chambers - 00:01:28 

It's great to be here. Looking forward to this. 

Jason Showard - 00:01:30 

Absolutely. Yeah. We're excited to have you as far as starting off with you. Where are you calling in from today? 

Adam Chambers - 00:01:36 

So today I'm speaking to you guys from the conference room here at Delta Separations in Cotati, California, just north of San Francisco and south of Santa Rosa. It's the main headquarters for Delta Separations and it's where we've been full time for the last couple of years and has been our home, this acquisition, and this strange year that we've had. 

Jason Showard - 00:01:59 

OK, great. Tell me a little bit about your journey to Delta and how you ended up working there. 

Adam Chambers - 00:02:06 

Of course, I don't think it would be uncommon to say that a lot of the people here at Delta, their route to the company was somewhat unconventional and I'm no exception. I studied forensic molecular biology, got a minor in chemistry and physics at the Virginia Commonwealth University. After graduating, I moved back over to Europe. I am half British in case that's of any consequence. And my father lives in Mediterranean Spain. I spent a couple of years up there just kind of figuring out what I was going to do. 

Adam Chambers - 00:02:43 

And I was invited to open an ethanol extraction facility in Southern California and in Coachella. And so I, you know, two weeks later, I was on a plane. And I had, and that was where I'd...]]>Learn the tricks of the trade for centrifugal ethanol extraction. Jason talks to Adam Chambers of Delta Separations about how their CUP line of ethanol extractors are the best tool for extracting the most out of your biomass, as well as all the other equipment offerings Delta has released recently. Times, temperatures, and SOPs that Delta usually charges for training on are 'extracted' in this interview.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:11 

Hello and welcome to Episode three of The Modern Extractor, the podcast that focuses on the processes, equipment and science found in a cannabis extraction laboratory. I'm your host, Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post-processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the progress of material through a lab, following it from Cultivar to concentrate. 

Jason Showard - 00:00:39 

Last week we discussed how to select quality biomass to extract from. After listening back to the show, I feel like I said a lot about what could go wrong there and neglected to mention that forming great relationships with your local growers is the absolute best way to consistently get quality biomass. In the second half of last week's show, we talked to Bri Tolp from Futurola about how their shredders can get you to your ideal mill sites for extraction. It was a great show and definitely worth a listen if you haven't already. 

Jason Showard - 00:01:08 

This week takes us to the next stage, which is the extraction process. We've got Adam Chambers from Delta Separations on today to give us the latest from Delta, as well as breakdown how their revolutionary CUP Series centrifuges will get you the most out of your material. So without any further ado, Adam Chambers, welcome to The Modern Extractor. 

Adam Chambers - 00:01:28 

It's great to be here. Looking forward to this. 

Jason Showard - 00:01:30 

Absolutely. Yeah. We're excited to have you as far as starting off with you. Where are you calling in from today? 

Adam Chambers - 00:01:36 

So today I'm speaking to you guys from the conference room here at Delta Separations in Cotati, California, just north of San Francisco and south of Santa Rosa. It's the main headquarters for Delta Separations and it's where we've been full time for the last couple of years and has been our home, this acquisition, and this strange year that we've had. 

Jason Showard - 00:01:59 

OK, great. Tell me a little bit about your journey to Delta and how you ended up working there. 

Adam Chambers - 00:02:06 

Of course, I don't think it would be uncommon to say that a lot of the people here at Delta, their route to the company was somewhat unconventional and I'm no exception. I studied forensic molecular biology, got a minor in chemistry and physics at the Virginia Commonwealth University. After graduating, I moved back over to Europe. I am half British in case that's of any consequence. And my father lives in Mediterranean Spain. I spent a couple of years up there just kind of figuring out what I was going to do. 

Adam Chambers - 00:02:43 

And I was invited to open an ethanol extraction facility in Southern California and in Coachella. And so I, you know, two weeks later, I was on a plane. And I had, and that was where I'd kind of get my start. And in the middle of the Mojave, really hot, inhospitable environment but we threw together some shipping containers that we retrofitted ourselves. And did the electrical and all of that stuff. And fitted with our own homemade extraction system with pumps and some basic lab gear as a proof of concept before we were picked up as being, you know, after we proved what we could do. 

Adam Chambers - 00:03:28 

Langfield Global. The notable ethanol solvent supplier in general and Verano Holdings, that they decided to invest in us so we formed a new, that went from [inaudible 00:03:40] manufacturing, which was the original name to DGV Group, the conglomerate of the three companies to produce distillate at large quantities. And so we started to do research as to how we would be able to handle this throughput. And we came across Delta [inaudible 00:04:00] and our CEO met them at a trade show. And they were, you know, very, he was very enamored by the CUP series in general, as it should have been. 

Adam Chambers - 00:04:12 

And we made the decision to go to their gear and actually ended up with some of the very first, if not the first falling film and rolled film distillation units, as well as the CUP 30 that we had. And we also made a bit of a precursor makeshift version of the DC 40 or so, just with a keg, a heat exchanger, and some compressors outside. And all that again in shipping containers, individualized, but very, very well kept. We were a group that had all studied hard science in school and kind of knew what we wanted. 

Adam Chambers - 00:04:50 

And we worked out all of the S.O.Ps. The following film that and the chiller designated to it does not [inaudible 00:04:58] not quite robust enough to keep up with 128-degree heat in the summer. 

Jason Showard - 00:05:04 

I could imagine that. 

Adam Chambers - 00:05:06 

Yeah, it was rough. So we helped Delta to find their way to G and D as a supplier for their trailers, that went rather well. And that's the falling film 60-gallon variant was also born just because they had more. The robusticity of the entire platform just kind of went up. And now while it was about a forty-five gallon capacity for us people. In a normal environment to push a bit more. Also hoped to make some modifications to the RFE. So one of us kind of came up with the [inaudible 00:05:39] helped them with the standard way to get a really good removal rate for cannabinoids and the CUP series. Involved in that project were many of the different people at Delta because we were kind of the canary in the coal mine for a lot of their newer platforms. 

Adam Chambers - 00:05:55 

So I met Ben and Jim out here. Steven's being the founder and Jim being the head engineer. And obviously some of their more famous characters like John and Casey, who I owe a lot to. They taught me a whole bunch, and it made me a much better extractor. They have a lot of experience in the game. 

Adam Chambers - 00:06:15 

And then I, you know, I wasn't very happy after we completed all of this stuff, we weren't very much appreciated for our work. So I decided to move on. And I took a job with another company called Halo Labs that produced products for some reputable brands, Hush being one of them for instance. They did use hydrocarbons to extract and I helped them with some optimization that they needed in their labs. The head of when [inaudible 00:06:48] kind of crippled them a little bit and they were forced to let a bunch of people go. 

Adam Chambers - 00:06:54 

And that was when I finally made the right decision, hit Ben up for a job. And he, you know, with open arms helped me come up to Santa Rosa. And actually, yesterday is March [inaudible 00:07:09], the anniversary of when I joined up here. Just shortly before the acquisition and everything. It's been kind of strange. I've been involved with Delta for much longer than I've worked here, I suppose. Yeah, that's kind of the come to the company story for me here. 

Jason Showard - 00:07:28 

All right. Yeah, I am no stranger to how those relationships grow, and when you're one of the first people to receive some equipment, and they actually are good at giving feedback and having technical conversations, you can build some relationships really quickly. 

Adam Chambers - 00:07:44 

Yeah, and Ben is a visionary and a fantastic human being. It changed my life for the better as well. So I was happy to help him out when we were pioneering some of his gear. But more so when he offered me a job and was so generous with me. I just owe him a lot. 

Jason Showard - 00:08:05 

Nice. Well, that's great. So can you give me a brief, like a bird's eye view of Delta as a company? How did they start? How did it all come about? 

Adam Chambers - 00:08:16 

Yeah, of course. So, again, it comes down to Ben really. Ben's been in the game for a long time. Longer than I've even considered it an industry before legalization, all of that good stuff. He is a technical man himself. 

Adam Chambers - 00:08:34 

But this started out, you know, I suppose you could say that Delta was kind of founded on his just, services in building some custom systems. Despite the fact that ethanol is the main, what Delta is known for. Ben also has experience building CO2 and hydrocarbon systems, along with some of the other people that he helped start Delta with as well. They're also to be credited. 

Adam Chambers - 00:09:02 

And as it progressed, you know all those five years ago or so, around three years ago, that is when Ben had the bright idea to make an ethanol [inaudible 00:09:13] that would go two directions. And it sounds simple, but the electrical engineering work that goes behind a motor that can do that readily is harder than you might think. And so they came up with a method and optimized it, paid for it. And lo and behold, it just works better than most anything else out there. 

Jason Showard - 00:09:32 

I can attest to that. Absolutely. Yeah. That's why when it came down to the episode on centrifugal extraction, I was like, OK, Delta is the one that I want to talk to. I was very happy to get you on the phone. 

Adam Chambers - 00:09:45 

Yeah, very happy to talk about. 

Jason Showard - 00:09:47 

Yeah, I mean, you guys got to be proud of being the best. 

Adam Chambers - 00:09:51 

Yeah. I mean, I feel bad repping it. I guess it helps that the [inaudible 00:09:57] I suppose helped in developing it, but the engineers that developed it are the real rock stars. 

Jason Showard - 00:10:02 

Right on. So Delta started doing ethanol extraction and that was their main bag. When I got into the industry, every manufacturer had their specialty. You went to Delta for your centrifuge and there are other manufacturers that you would go to for a falling film or road evap even before that. And then moving on to all the various stills that are out there for distillation. Nowadays, everybody is coming out with their own entire suite. So can you give me a brief description of just the current equipment offerings that you guys have now beyond the CUP series centrifuges? 

Adam Chambers - 00:10:48 

Of course. So as far as just Delta is concerned because obviously, we have under the Gibraltar umbrella as of this year and everything. With specific to Delta or the ethanol products and again, the rolled film molecular distillation rate that we offer. But it gets [inaudible 00:11:11] from the beginning, so to speak, the Direct Chiller 40, DC 40, as it's known, is a [inaudible 00:11:19] filtering system that will allow you to feel, it's very important and very useful, I guess, in the sense that it can one, chill your ethanol and has its onboard pump to bring in solvent from a tertiary location, but it can also refill your [inaudible 00:11:37]. That's one thing that's really cool, that it's so you can run things in a loop. We offer, we're partnered with [inaudible 00:11:45] to provide a filtration skill that again has its pump on it. So that you can make sure that after it comes up [inaudible 00:11:54] CUP 30. 

Jason Showard - 00:11:55 

I'm sorry, I didn't hear, I didn't hear which, what company that was for the filter. 

Adam Chambers - 00:12:00 

Oh, it's ErtelAlsop 

Jason Showard - 00:12:02 

OK. 

Adam Chambers - 00:12:03 

Yeah, they're a fantastic filter manufacturer for [inaudible 00:12:06] filtration and beyond the, you know. If you've processed before you've ever tried to use vacuum filtration for cannabis processing, you've probably had a really bad time. 

Jason Showard - 00:12:18 

It is not fun. 

Adam Chambers - 00:12:20 

Nah! That used to be my entire day way back when. And so yeah between that and winterization. I was very thankful when we realized that we wanted to go cold and that you could push your miscella through a filter instead of having to pull it through and wait several hours longer than it took it to attack your material. So, yeah, that compresses our extraction suite. Like the loop there, that you can do, and you can [inaudible 00:12:51] as many bags as you can fit into a batch of ethanol. That it was ever going to take it out of the loop, which we're very happy with. 

Adam Chambers - 00:12:59 

Afterwards, you can send it out to our falling film evaporator. It comes in two different, you can call them models the steel there is the same. And it's just a chiller size variant that will give you two different capacities of forty-five or six pounds an hour. Should be expecting some higher throughputs in the future, the near future that is. As it stands, we're implementing some new technology. My engineers will come and sock me if I talk too much about that, to get some higher numbers for the evaporation tech that we have. But the falling film is just the best way to go about it when you're extracting botanical compounds with ethanol. 

Jason Showard - 00:13:46 

Couldn't agree. 

Adam Chambers - 00:13:47 

Pull over a lot of. Yeah, exactly. You'll pull over a lot of water and stuff. And the falling film, the way that it's laid out, just re-proofs each time so you can pick all of the moisture content out of there. 

Jason Showard - 00:13:59 

OK, actually, I wasn't planning on getting too deep into this today because it is an episode on centrifugal extraction. But you've piqued my interest with the reproofing on your falling film. If you could just real quick describe why it reproofs the ethanol. I'd love to know. 

Adam Chambers - 00:14:21 

Yeah, of course. So as it falls down the column, the extract that is [inaudible 00:14:27] you vaporize it and the extract stays in its, you know, the viscous solid form, it's going to fall into the column, down the column and be recollected. But the vapor passed on the other hand, is such that it goes through a couple of ducts and travels against gravity to travel back to the second side of the heat exchange, the plate heat exchangers where that are being chilled. And will thus re-condense the ethanol. The molecular weight of water and any of the trapped extract as it's coming through across that column, is going to it's going to drop out against gravity effectively. And just be re-collected into the concentrate where you can easily get rid of it with the heat which [inaudible 00:15:18] 

Jason Showard - 00:15:20 

OK, that makes sense. So it stays with the heavies, so to speak. 

Adam Chambers - 00:15:24 

Exactly. 

Jason Showard - 00:15:24 

That's interesting. OK, cool. Was that it for your equipment offerings? Oh. No you guys have your molecular [inaudible 00:15:33] as well. 

Adam Chambers - 00:15:34 

Yeah, exactly. There's the roll film which we really, I really like. You know, it's, I love Delta Separations, but I'm sure anybody here would admit as well, it's a great machine for the price point. That again, you can do it, I love [inaudible 00:15:50] units, and there are plenty of other units out there that have a great price tag but are absolutely phenomenal in operations. [inaudible 00:15:58] yield as well, for a five-liter unit. It's hard to beat. [inaudible 00:16:04] it’s always nice to have because they won't break like the wipers will, if you've ever again, just going back to the processing days. If you've ever had to stop pulp production to change the wipers on a wiped film unit, can be really frustrating. 

Jason Showard - 00:16:20 

Well, and then also with the wiped film units, if you don't change them and nothing catastrophically goes wrong, they just recede and then you're slowly and slowly getting less temperature control as that film builds up a little bit thicker. It's something that's a little bit insidious there. Where nothing's catastrophically wrong, so you don't go in to fix it. But then it ends up costing you yield for sure. 

Adam Chambers - 00:16:43 

Exactly. And I'd say that I think there's one other machine that is worth mentioning. We've recently this year released our Vortex Trichome Separator. Our solventless [inaudible 00:16:59] hash machine. That's co-developed with [inaudible 00:17:03] it uses a patented dual vortex that's generated by the paddles down at bottom of the basin to, again, just kind of whip a vortex into the water and brush the trichomes off very gently to create some fantastic water hash with it as well. 

Adam Chambers - 00:17:24 

And it has some nice safety features and a [inaudible 00:17:27] pump to be able to pull your water throughout and not have gravity drain it as the older prototype units. That's all...]]>d3d98b66-c079-47ce-86a4-f7d19e291cb0Tue, 05 Jan 2021 09:00:00 -070053:09nofull13Jason ShowardS1 E02 - Cannabis Biomass Selection And Extraction PreparationLearn the tricks of the trade when it comes to selecting the highest quality biomass and preparing it for extraction. Jason talks to Bri Tolp of Futurola about how their shredders are the best tool for getting to your ideal mill size.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to Episode two of The Modern Extractor, a podcast focusing on the processes, equipment, and science found inside a cannabis extraction lab. I'm your host, Jason Showered, and I work professionally in the cannabis extraction field. If you've listened to any of the previous shows, you know that season one is focused on ethanol extraction and post-processing. And each episode focuses on a particular stage in that process following the material through the lab from start to finish. If you haven't listened to any of the previous shows, welcome to the Modern Extractor. 

Jason Showard - 00:00:40 

In today's show, we'll be talking about how to select the right biomass for extraction, as well as how to prepare that biomass for the most efficient extraction possible. We'll have Bri Tolp from Futurola on with us later in the show to talk about how their shredders are the best tool to get you to your ideal mill size. But first, let's talk a bit about how to find good material to extract from. Obviously, the easiest way to do this is to get a sample, send it to a lab, wait for the results, and then purchase material that meets the right cannabinoid concentration specs for whatever you're trying to produce. 

Jason Showard - 00:01:12 

In a perfect world, there would always be time for this and it's absolutely how it's done for the large-scale industrial operations. It's really important to buy this way if you're a CBD producer buying hemp, so that you can ensure the material is not too high in THC content. Buying hot hemp could actually cost you more in chromatography to remediate the THC from the final product than the CBD will be worth in the end. There isn't always time to wait for lab results in the procurement process. 

Jason Showard - 00:01:38 

And this is where an experienced eye can make a big difference in your bottom line. If you're at the scale where you're extracting a thousand pounds or more weekly, it's unlikely that all your biomass is coming from the same farm all year round. That means that there's likely to be a broker involved who is collecting from a bunch of different farms to sell to extractors. With that being the case, there are often many different batches of biomass added to one load. 

Jason Showard - 00:02:00 

Hopefully they're separated, often they aren't. Hopefully the broker will tell you the story behind the load, but well, brokers. And even if you trust your broker, he could have been misled. So a thorough inspection isn't rude. It's just good business. First things first. We're going to look at all the different bags. The actual physical bags that the material's inside of. Not every farm packs their material up the same way. Not every store sells the same bags. 

Jason Showard - 00:02:26 

Is there any tape on any of the bags? How are they closed or tied? This will be our first clue as to whether or not there are multiple batches in the load. If there does appear to be multiple batches, we're going to want to open and inspect a couple of bags from each. Dig down past the top and into the middle of the bag. Get a good handful, pull it out, palm up, give it a good squeeze in your hand and then let go. 

Jason Showard - 00:02:48 

Good material will stick together when you let go and keep the...]]>Learn the tricks of the trade when it comes to selecting the highest quality biomass and preparing it for extraction. Jason talks to Bri Tolp of Futurola about how their shredders are the best tool for getting to your ideal mill size.

EPISODE TRANSCRIPT:

Jason Showard - 00:00:10 

Hello and welcome to Episode two of The Modern Extractor, a podcast focusing on the processes, equipment, and science found inside a cannabis extraction lab. I'm your host, Jason Showered, and I work professionally in the cannabis extraction field. If you've listened to any of the previous shows, you know that season one is focused on ethanol extraction and post-processing. And each episode focuses on a particular stage in that process following the material through the lab from start to finish. If you haven't listened to any of the previous shows, welcome to the Modern Extractor. 

Jason Showard - 00:00:40 

In today's show, we'll be talking about how to select the right biomass for extraction, as well as how to prepare that biomass for the most efficient extraction possible. We'll have Bri Tolp from Futurola on with us later in the show to talk about how their shredders are the best tool to get you to your ideal mill size. But first, let's talk a bit about how to find good material to extract from. Obviously, the easiest way to do this is to get a sample, send it to a lab, wait for the results, and then purchase material that meets the right cannabinoid concentration specs for whatever you're trying to produce. 

Jason Showard - 00:01:12 

In a perfect world, there would always be time for this and it's absolutely how it's done for the large-scale industrial operations. It's really important to buy this way if you're a CBD producer buying hemp, so that you can ensure the material is not too high in THC content. Buying hot hemp could actually cost you more in chromatography to remediate the THC from the final product than the CBD will be worth in the end. There isn't always time to wait for lab results in the procurement process. 

Jason Showard - 00:01:38 

And this is where an experienced eye can make a big difference in your bottom line. If you're at the scale where you're extracting a thousand pounds or more weekly, it's unlikely that all your biomass is coming from the same farm all year round. That means that there's likely to be a broker involved who is collecting from a bunch of different farms to sell to extractors. With that being the case, there are often many different batches of biomass added to one load. 

Jason Showard - 00:02:00 

Hopefully they're separated, often they aren't. Hopefully the broker will tell you the story behind the load, but well, brokers. And even if you trust your broker, he could have been misled. So a thorough inspection isn't rude. It's just good business. First things first. We're going to look at all the different bags. The actual physical bags that the material's inside of. Not every farm packs their material up the same way. Not every store sells the same bags. 

Jason Showard - 00:02:26 

Is there any tape on any of the bags? How are they closed or tied? This will be our first clue as to whether or not there are multiple batches in the load. If there does appear to be multiple batches, we're going to want to open and inspect a couple of bags from each. Dig down past the top and into the middle of the bag. Get a good handful, pull it out, palm up, give it a good squeeze in your hand and then let go. 

Jason Showard - 00:02:48 

Good material will stick together when you let go and keep the same basic shape it was when it was squeezed in your hand. We call this the squeeze test. After the squeeze, rub it together between your hands like you're warming up at a fire. See how crumbly it is. If it turns to dust, it's not ideal, but it'll still work if it passed the squeeze. The best-case scenario is that it breaks a little, but still some moisture content. 

Jason Showard - 00:03:09 

So it rolls around and compresses and sticks to your hands a little instead of powdering. Leaving a little of what you just rolled around in your hands. Bring both hands up to your face and get your face down in there. You know what smell you're looking for. One thing to pay attention to with the smell test is the presence of any alcohol or solvent odors. Keep your eyes open when you get your face down into your hands to give it a smell. 

Jason Showard - 00:03:30 

If your nose misses it, your eyes may water a bit in the presence of solvents. While the industry is slowly cleaning itself out and the honorable business folks are rising to the top, there are certainly some bad actors out there still in the mix. Some rascally brokers have even been known to sell material that's already been processed. This is referred to as Spun Trim. If it appears to have been processed with alcohol in a centrifuge or Blown Trim if it appears to have been run through a hydrocarbon column. I've even seen some “fresh trim” come in that still holds the shape of the column it was processed in. 

Jason Showard - 00:04:04 

This will look like little biomass hockey pucks that are usually three to six inches in diameter. There are some vapor probes you can buy for this, but I find them less reliable than these inspections. As you process material, pay attention to what your own processed material looks and feels like after it's had a chance to dry out. If it looks and acts like that, don't buy it. OK, so we've got our hands on some good quality biomass. Our lab tests came back at 12 percent. 

Jason Showard - 00:04:29 

It squeezes and smells nice and sticks to our hands and it's going to make some beautiful goldies. The next step in ensuring we get everything we can out of this material, is to make sure that it's milled to the ideal particle size. There's a bunch of machines out there that say they do this the best, and many a booth full of promises at BizCon. Extractors use everything from shredders to hammer mills, to mulchers, blenders, food processors, you name it. If it chops things up, we've tried it. 

Jason Showard - 00:04:56 

If there's one thing not lacking in this community, it's innovation and willingness to think outside the box. For about a hundred bucks at your favorite big box hardware store, you can get a Toro mulcher that'll do the trick. But it's a bit of a pain to use. When you run it forward, it's a leaf blower that blows air, and in reverse, it's a mulcher that sucks material through the metal fan blade and mulches it into a collection bag. Unfortunately, if the material's dry, it powders it up pretty well, even on the lowest setting. When the time comes to invest in a machine that mill as fast and accurately as possible, look no further than a Futurola shredder. 

Jason Showard - 00:05:29 

When choosing your desired mill size. There's a lot of factors to consider. Mill it too fine, and it will break more cell walls in the material, allowing for more chlorophyll and undesirables to be extracted. The finer the particle size, the more ethanol will be retained in the biomass after the spin cycle of your centrifugal extraction. After a run through the centrifuge, all of the ethanol that is retained in the biomass, is not only a loss of ethanol, but a loss of desirable oil that you've just dissolved into the ethanol. 

Jason Showard - 00:05:59 

This ethanol retention loss issue is often compounded by the fact that the same batch of ethanol is regularly re-chilled and used to extract from multiple batches of biomass, before being run through an evaporator and having the oil separated out of it. The process of evaporation and ethanol recovery is often a lab's biggest bottleneck. So it's a current industry standard to use one batch of ethanol to extract from multiple batches of biomass. From a solubility standpoint, there's probably room to dissolve seven or eight batches of biomass into the ethanol. 

Jason Showard - 00:06:30 

But your loss rate from the ethanol retention in the spun biomass would make this inefficient. The correct mill size for your extraction recipes is critical. You'll be able to extract slightly more with a smaller mill size because the ethanol will be able to make contact with more of the surface area of your biomass in the centrifuge. But more of the ethanol will be lost to retention in your biomass after the spin cycle. Your particle size decision should be made based on the following factors. 

Jason Showard - 00:06:57 

One, what is your evaporation capacity? If you can run your ethanol through one bag of biomass and send it off to evaporation without bottlenecking yourself at the evaporation stage, this is the best way to minimize loss of oil. However, if this is the case, you'd probably be better off buying an additional centrifuge and figuring out how to send miscella that has two or three passes on it to the evaporator. 

Jason Showard - 00:07:19 

Two, what is your cost of ethanol? If you're paying a premium for ethanol, then the ethanol loss in finely milled material will start to add up. It isn't going to make or break your operation, but it is one factor to consider when making mill-size decisions. Cost-cutting is going to become a bigger factor, with the industry heading towards larger, more streamlined operations producing more product. 

Jason Showard - 00:07:42 

Three, what is the cost and accessibility of your biomass? If you can get biomass readily and inexpensively, then the extraction efficiency may not be as important as it would be if you were paying a premium for it. If this is the case, larger particle size, that may leave a small amount of desirables behind, but won't retain as much ethanol, may be ideal. 

Jason Showard - 00:08:02 

Four, what is the demand for your finished goods? If there's an infinite demand for your finished product and as soon as it's produced, it's out the door. The goal should be to produce as much as possible, as fast as possible. That said, it may be worth the retention loss, to run your ethanol through more bags of biomass than you otherwise would so that your miscella is as rich as possible. 

Jason Showard - 00:08:23 

This will decrease evaporation time and increase your gross output. If three or more bags will be run on one batch of ethanol, keeping the mill size between a quarter-inch and five 16th inch is ideal. In my experience, a quarter-inch particle size and two centrifuge runs, on one batch of ethanol was ideal after plugging in answers to the above questions. Depending on your variables, a range between three 16th and five 16th of an inch particle size is the sweet spot. 

Jason Showard - 00:08:50 

If you're running sugar leaf trim, larger particles are OK because they aren't dense. If your biomass has dense flower in it. Smaller particles are better. The idea is to make sure the ethanol has the ability to easily flow around all the surface area of your material. Sometimes the ethanol won't penetrate and extract from the center of dense snugs if they're left too large. After your materials build to your chosen particle size, it's time to back it up for your centrifuge. 

Jason Showard - 00:09:16 

Centrifuge bags are typically made from a light nylon mesh sewn into a tube with a flat bottom and a flat zippable top. These bags allow for ethanol to flow freely through your biomass and dissolve the compounds you're extracting. But they keep all the biomass contained so that it can easily be removed from the centrifuge after it's been extracted. Examine your bags regularly and be prepared to retire bags that have holes in them. Your downstream filters will definitely thank you. It's worth noting here that if you've done a good job milling your material, there will be less stems to poke holes in your bags and they'll last longer. 

Jason Showard - 00:09:49 

Well, now that we've gone over how to select your biomass and how to choose your ideal mill size, let's talk to Bri about how Futurola's shredders could help you get there. 

Jason Showard - 00:09:57 

The Modern Extractor would like to welcome guest Bri Tolp of Futurola to the show. Welcome. We're happy to have you here today. 

Bri Tolp - 00:10:03 

Thanks, Jason. I'm happy to be here. 

Jason Showard - 00:10:06 

So Bri where are you calling in from today? 

Bri Tolp - 00:10:08 

I am calling in from sunny Los Angeles where we are, you know, in lockdown. 

Jason Showard - 00:10:15 

I am also in the Los Angeles area, and also under lockdown. But hey that gives us plenty of time to talk about Futurola. So give me a bird's eye view. Tell me what you guys do as a company. 

Bri Tolp - 00:10:25 

So Futurola actually started in '96 in Amsterdam. We were a Futurola coffee shop. Funny enough. And if you go there now you'll see Futurola rolling papers and everything in all the different coffee shops all over Amsterdam. When we first started, though, we were focused more on the consumer side of things. You know, so we did rolling papers, grinders, these really incredible hand rollers that are just really simple and easy to use. Once we decided to bring it to the US, we started pushing that same market here, grinder's, rolling papers, all these different accessories. 

Bri Tolp - 00:11:00 

But going to all these trade shows and talking to all these different companies, we realized there was, that there was really something that was lacking here. That there's all these people that are, they're producing pre-rolls and they're doing all these different things, but they don't have a solution for it. So we started building the brand, and we started coming up with ideas to make things easier, streamlined and just better for production. That's when we created the cones. That's when we came out with the Knockbox, which is the machine that does a hundred pre-rolls in two minutes, which we actually just released a new one that does three hundred in two minutes. 

Bri Tolp - 00:11:34 

That's when we developed the first shredder, which I know we'll touch base on this, you know, shortly. You know, so we really went from this consumer side of things to more of now business to business now. Where we're working with these companies to help them fulfill their pre-roll needs. 

Jason Showard - 00:11:51 

Nice. So how did the Futurola's material prep products for pre-rolls become a staple of extraction lab material prep? How did that all come about? 

Bri Tolp - 00:12:02 

So we've, we created our first shredder in 2016, and the reason why that came about is because we had, right, so we had the lockbox. So we have this incredible, easy to use, extremely affordable piece of equipment that's going to produce a hundred pre-rolls in two minutes. But we don't have a solution for them to grind up their product you know. I don't know if you know this, but I'm sure everyone listening will understand, the way to grind a product was a food processor. It worked great. It's dandy. It's cheap. You have them at home. They're easy to get. But the problem with that is that you're not getting a consistent grind. So when people were using that with the machine, they're getting powder at the bottom, thicker material at the top. And when they're using it to run in the Knockbox, it's giving them inconsistent fills. 

Bri Tolp - 00:12:49 

So they're like, you have this incredible machine, why don't you have something to go along with it? And that was really when we created the shredder and from doing that. So I joined the team in 2018 and I worked at all these different groves across California. And our first shredder that we came out with, was basically an empty barrel with almost like, they're specialized weed whacker whips. They're moving on extremely quick speed to grind up the material. It's all based on time. 

Bri Tolp - 00:13:23 

So it's about two to seven seconds on average to grind up anywhere from one to seven pounds. But it's all based on time. So depending on the time you set and the material you're working with, that'll give you different material size. Now, when I came in, we had just released the super shredder. The super shredder is the unit that has a screen built into it. That's this three millimeter screen. So that screen is going to separate the stems and separate any other thicker piece of material that you don't want in the pre-roles. 

Jason Showard - 00:13:57 

Is that super shredder the most popular one used in extraction prep? 

Bri Tolp - 00:14:03 

Yes. And the reason being because when a lot of companies that are processing material for extraction, I mean, there's all different types of material that they're using right. But for the most part, they're getting a lot of biomass. And it's not like it's just clean, beautiful pieces of broken-down material. It's, there's sticks, there's stems. There is, it needs to be cleaned up. So by being able to process it with this screen in there, that screen is separating the sticks and the stems from the good product that you want to use. So there's no other sifting process needed after. And like I said, you're doing this in two to seven seconds. 

Jason Showard - 00:14:40 

Let me stop you for a second here. What I like to try to do is when we're talking about a machine on the show, I like to picture my listeners driving or not in front of a computer so they can't just click on and see what it looks like. So let's give a description of, you said the super shredders the one that's the most popular for extraction. So, let's describe the, can you describe the whole...]]>7137f1d4-72a4-4f90-8433-b5988d9fda12Tue, 29 Dec 2020 08:00:00 -070036:51nofull12Jason ShowardS1 E01 - Cannabis Extraction And Post Processing OverviewJason Showard walks listeners through an overview of the extraction, distillation, and crystallization processes used to take cannabis from cultivars to concentrates.

Episode Transcript:

Hello, and welcome to the modern extractor. I'm your host, Jason Showard. And I work professionally in the cannabis extraction field. After years of experimentation tens of thousands of dollars in lab tests to collect data from those experiments, and hundreds of thousands of pounds of biomass successfully extracted and distilled. I decided to spill my secrets to you with this podcast. The modern extractor will be focusing on the processes, equipment and science found inside a cannabis extraction laboratory. I've yet to find a curated collection of extraction knowledge, and that's exactly what I'm going to build here. I decided to produce this podcast because I kept looking for something like it to listen to, and it just didn't exist. In Season One, we'll be focusing on ethanol extraction and post processing and either distillate or isolate. The shows will be released in an order which follows the workflow of material through a lab. Each episode will dig deep into a particular stage in that workflow and discuss the various approaches with industry expert guests. In today's show, we'll be taking a bird's eye view of the entire ethanol extraction and post processing workflow. For the sake of simplicity, and getting through the whole process in one show, this will be a less technical overview of the full process. For this overview, I'll be following what I believe to be the best approach to ethanol extraction. in future episodes, we'll dig deeper into each of the stages and pick apart the different options and approaches a lot more technically, think of this as both a walk through the process and a syllabus for what lies ahead in season one.

So after this week's overview, next week, in Episode Two, we'll talk about sourcing biomass and prepping it for extraction. The first step in any extraction operation is getting your hands on good material to extract from. Obviously, the ideal situation is to get a sample of the material you're interested in buying, send it to a lab and have the seller agree to hold the material for you until the test results come back and tell you exactly how much of each cannabinoid is present before you buy it. But this is a fast moving field. And there may not always be time for a lab test. You don't want to miss out on a good opportunity. But you also don't want to get burned by buying bad material. We'll go over some tests that you can do to ensure you're buying high quality fresh material that hasn't already been processed. After you've sourced your biomass, it's time to prepare it for extraction. The first step in the preparation process is either milling, shredding or grinding your material. It's just not efficient to extract from biomass that hasn't been appropriately broken up. There's no magic spec when it comes to mill size and your decisions here should be based on variables specific to your extraction operation. And Episode Two, we'll go over how to determine your ideal mill size based on variables unique to you, such as your evaporation capacity, your cost of ethanol, because the biomass, your access to biomass, and the amount of demand there is for your finished goods. Once you determine what your mill size will be, there are a lot of options out there to mill grind or shred your material down to spec. After trying way too many options. I landed on Futurola shredders to do the job right. On next week's show we will have Bri Tolp from Futurola as a guest to discuss how Futurola shredders will get you to your desired mill size better than the competition. After your material has been milled down, it's time to bag it up for extraction. Most centrifuge manufacturers sell specially constructed nylon bags that zip shut and fit their centrifuges perfectly. Once...]]>Jason Showard walks listeners through an overview of the extraction, distillation, and crystallization processes used to take cannabis from cultivars to concentrates.

Episode Transcript:

Hello, and welcome to the modern extractor. I'm your host, Jason Showard. And I work professionally in the cannabis extraction field. After years of experimentation tens of thousands of dollars in lab tests to collect data from those experiments, and hundreds of thousands of pounds of biomass successfully extracted and distilled. I decided to spill my secrets to you with this podcast. The modern extractor will be focusing on the processes, equipment and science found inside a cannabis extraction laboratory. I've yet to find a curated collection of extraction knowledge, and that's exactly what I'm going to build here. I decided to produce this podcast because I kept looking for something like it to listen to, and it just didn't exist. In Season One, we'll be focusing on ethanol extraction and post processing and either distillate or isolate. The shows will be released in an order which follows the workflow of material through a lab. Each episode will dig deep into a particular stage in that workflow and discuss the various approaches with industry expert guests. In today's show, we'll be taking a bird's eye view of the entire ethanol extraction and post processing workflow. For the sake of simplicity, and getting through the whole process in one show, this will be a less technical overview of the full process. For this overview, I'll be following what I believe to be the best approach to ethanol extraction. in future episodes, we'll dig deeper into each of the stages and pick apart the different options and approaches a lot more technically, think of this as both a walk through the process and a syllabus for what lies ahead in season one.

So after this week's overview, next week, in Episode Two, we'll talk about sourcing biomass and prepping it for extraction. The first step in any extraction operation is getting your hands on good material to extract from. Obviously, the ideal situation is to get a sample of the material you're interested in buying, send it to a lab and have the seller agree to hold the material for you until the test results come back and tell you exactly how much of each cannabinoid is present before you buy it. But this is a fast moving field. And there may not always be time for a lab test. You don't want to miss out on a good opportunity. But you also don't want to get burned by buying bad material. We'll go over some tests that you can do to ensure you're buying high quality fresh material that hasn't already been processed. After you've sourced your biomass, it's time to prepare it for extraction. The first step in the preparation process is either milling, shredding or grinding your material. It's just not efficient to extract from biomass that hasn't been appropriately broken up. There's no magic spec when it comes to mill size and your decisions here should be based on variables specific to your extraction operation. And Episode Two, we'll go over how to determine your ideal mill size based on variables unique to you, such as your evaporation capacity, your cost of ethanol, because the biomass, your access to biomass, and the amount of demand there is for your finished goods. Once you determine what your mill size will be, there are a lot of options out there to mill grind or shred your material down to spec. After trying way too many options. I landed on Futurola shredders to do the job right. On next week's show we will have Bri Tolp from Futurola as a guest to discuss how Futurola shredders will get you to your desired mill size better than the competition. After your material has been milled down, it's time to bag it up for extraction. Most centrifuge manufacturers sell specially constructed nylon bags that zip shut and fit their centrifuges perfectly. Once filled, the bags of biomass should be held at your desired extraction temperature for about eight hours.

In episode 3 we'll get into the extraction process. It's time to decide what temperature we want to run our extraction. Room temperature extraction will ensure we extract the most from our biomass but along with maximizing the extraction of desirables we also extract far more undesirables than with a cold extraction. If done correctly, cold extraction will leave a very small percentage of desirables behind, but reject so many of the undesirables that it will allow us to skip cumbersome downstream processes like winterization and carbon filtration. Cold extraction requires pre shelling of both our ethanol and our biomass. I'm a big proponent of this method, but in Episode Three, we will break them both down and discuss why it may be correct to choose one over the other as well as ideal run temperatures and some low tech chiller hacks to save some money until you're ready to buy that chiller. The majority of ethanol extraction is done in centrifuges, only micro garage scale or huge high throughput CBD labs use other methods. While we may touch on some of the other methods out there, we'll be focusing primarily on centrifugal extraction. An extraction centrifuge is basically an explosion proof stainless steel washing machine that's optimized to agitate and extract cannabis. A typical centrifuge run will look something like this. Get your biomass to your extraction temperature for about eight hours, get the ethanol down to the extraction temperature. Put the bagged biomass into the centrifuge, push or pumped chilled ethanol into the centrifuge, run the agitate cycle, run the spin cycle and then drain the ethanol which now contains oil. Often, extractors will get the same batch of ethanol back down to extraction temperature and run it through a second, third, or even fourth bag of biomass. This is another decision that is directly dependent on your operation variables. We will get into picking all this apart with our guests Adam Chambers of Delta Separations. Delta is the creator of the first extraction centrifuge to hit the market and has become quite a beast in the industry. With his extraction experience and education in forensic biology. Adam is super knowledgeable on the entire process, and I'm excited to have him on the show.

Moving on to Episode Four, we'll tackle filtration. I can't stress the importance of filtration enough, trust me, having effective stage filtration processes makes life so much easier and reduces the wear on your equipment. So at this point in the process, we've run our ethanol through two or three bags of biomass. What we have now has many names, tincture, masella mother liquor, the list goes on. Technically, I think masella is the correct term. But you'll catch me saying tincture here and there as well. Old habits die hard. It's It's funny how the terminology you use in your first lab will stick with you forever, get me around my original crew and we have some ridiculous names for everything. You'll catch me peppering them in here and there. Anyway, back to filtration. Some particulate matter will always break free from the biomass during the extraction agitation. The majority should be retained in your nylon centrifuge bags with some amount always get through and be suspended in our solution. All of our downstream equipment is depending on us to get the particulate as well as any fats, waxes and lipids extracted from the plant out of solution. If we're running cold, we likely haven't extracted too many of the fats, waxes and lipids. But it is important to get our miscella filtered well it's still called as these components are more easily filtered out at the lower temperatures. medium scale operations typically put together or purchase a filters skid. In my experience. The best configuration here is a bag filter, sometimes two in series staged in mesh size, feeding into a one micron lenticular filter. We'll have Maria Peterson from Scott laboratories join us in Episode Four to discuss the ins and outs of the many different styles of filtration used in cannabis extraction. She's the most knowledgeable person I've ever spoken to about filtration and I'm really happy I get to share her with you guys. Let's catch back up with our work in progress. After running our ethanol through a few bags of biomass and filtering the miscella, it's now time to separate the oil from the ethanol.

Episode Five takes us into evaporation solvent recovery and reproofing. So far, we've extracted the oil from the plant, but it's currently dissolved in ethanol at a very low ratio. In order to continue processing the oil the ethanol has to be removed. This part of the process has certainly come a long way. In the beginning, people were boiling ethanol off of their extracted oil on a hot plate. This is definitely not efficient, definitely not scalable and just plain dangerous. From there, rotary evaporators became the standard tool to separate the oil from the ethanol. While they were a significant safety improvement from a hot plate, rotovaps just weren't fast enough and bottlenecked many an extraction operation. Then along came falling film evaporators! These completely changed the solvent recovery game, with one unit being able to replace about 10 rotovaps. Trusteel was one of the first if not the first company to design a falling film evaporator for extractors. Thanks to their AUTOVAP line, ethanol extraction became much more scalable. Falling film evaporators are now the industry standard solvent recovery device. In Episode Five, I'm very excited to have Ray Van Lenten, founder and CTO of Trusteel on the show to discuss how falling films work and why they're the best solution for solvent recovery. For the sake of today's overview, the important thing to know about the falling film is that its function is to separate the cannabis oil from the ethanol that it's dissolved in. There are typically two collection vessels, one for the oil that's had the majority of the ethanol removed from it now referred to as crude, and one for the ethanol that's been vaporized off, re-condensed and collected again for future use. Before we follow the crude on to the next stage, it's important to note that during the extraction process, the ethanol can pick up water, it picks it up from the plant material and even from exposure to the air in the room. The ethanol and water from azeotropes that are hard to break. The azeotropes have a boiling point close to that pure ethanol, so they can't be separated out with any of the equipment we've discussed so far. As the proof of the ethanol decreases with the addition of water, the extraction efficiency also decreases. Medium to large scale operations will usually reproof the ethanol, removing the water and azeotropes with the molecular sieve or a multi plate fractional distillation column. At small scale, it's just not worth investing in the extra equipment. But at any real scale it's critical to reproof your ethanol and ensure you're getting the maximum extraction efficiency.

So back to our work in progress. We have crude oil... now what? In episode six we'll get deep into decarb with our guests Greg Arias of Aftermath Laboratories. Greg's a chemical engineer who you can usually find working on formulations, various cannabis chemistry projects or consulting of some sort. He's also my first phone call when I realize I need to call on the big guns for problem solving or brainstorming. Decarboxylation is the only chemical reaction that occurs during the entire extraction, distillation and crystallization processes. In the Decarb step, we will break the bond attaching the carboxylic acid groups to the cannabinoids through a timed exposure to heat. The majority of the THC and CBD found in a cannabis plant are found in their acidic forms of thca and cbda. thca is not psychoactive and won't produce the desired effects unless you decarboxylate it and convert it into delta 9 THC, which is psychoactive. CBDA has gotten a little bit more attention lately, and neither CBD nor CBDA are psychoactive. So occasionally the CBDA heavy hemp crude will be collected pre-decarb, but more commonly the hemp crude gets decarbed, distilled, and then crystallized into CBD isolate. A typical Decarb setup is a sealed jacketed pressure vessel with a mixing motor and a cold trap. Heated fluid is circulated through the jacket for temperature control. The mixing motor mounts to the lid of the vessel and has a shaft that penetrates down through a bearing seal on the lid. There's a small propeller mounted at the bottom of the shaft to stir the crude inside the reactor. The cold trap will we condense any residual solvents that are vaporized at decarb temperatures and pressures. decarboxylation takes place when the oil is held at a certain temperature for a certain amount of time. In Episode Six, I'll give out my time and temperature SOPs which I've kept top secret for years. They're way faster and lower temperature than a lot of the information that's out there and they work great.

Episode Seven takes us to devolatilization, which is a mouthful, so we call it terp strip. We terp strip so that we can remove all the volatiles which have a lower boiling point than our sought after cannabinoids. We do this so that we can achieve a far deeper vacuum on the distillate run that follows the terp strip run. The deeper vacuum on the ensuing distillate run allows us to keep the temperatures on our equipment lower and results in less thermal degradation or cannabinoids. wiped film or rolled film distillation is by far the most efficient method for this stage. So while I will touch on short path, the majority of the SOPs discussed will be pertaining to wiped or rolled film distillation units. If decarb went correctly, there shouldn't be any residual solvents in our decarbed crude at this point. The remaining volatiles are mostly terpenes. And we'll remove them much the same way that we removed the ethanol from our miscella by vaporizing them from the crude and re condensing them elsewhere to separate, or strip, the terpenes from the terp-stripped crude. In this process, your decarbed crude oil is pumped from the wiped films heated feed tank into the top edge of the evaporator body. The evaporator body is heated to a specified temperature using a fluid filled jacket. A wiper unit containing multiple sets of flexible squeegee-like vertical wipers spins inside the evaporator body. The wipers make light contact with the heated inner wall of the evaporator body so that when your crude is pumped into the body, the spinning wipers squeegee it around the entirety of the inner wall. The thin film of oil created by the wipers is easily heated to the temperature of the hot wall, vaporizing any volatiles in the crude that will vaporize at or below the set temperature and pressure. The vapors created are condensed on a condenser that runs down the center of the evaporator body. The condenser has a separate temperature control bath that allows it to be set at a different temperature than the evaporator body temperature that allows the vaporize terpenes to re condense into a liquid and the distilled terpenes run down the condenser and into the distillate collection vessel. Gravity and small angled grooves on the wipers help the decarbed crude make its way down the hot evaporator body wall and into the residue collection vessel. along the way and the volatiles have been removed and it's now referred to as terp-stripped crude. Extensive cleaning and a slight reconfiguration of the machine are needed before the terp-stripped crude can be run again on our wiped film to create distillate. For the sake of both time and loss efficiency. it's advisable to build up enough decarbed crude to do a large terp strip run followed by a large distillate run. Cleaning between runs is time consuming, and more or less the same amount of loss occurs on every run, whether it's 5 liters or 500.

Episode 8 is what we've all been waiting for. By far the most gratifying part of the process. cannabinoid distillation. time to make some Goldie's. We will be using the same style wiped film distillation unit we used on the terp strip for the distillate run, this time by raising the temperatures on the evaporator body and main condenser as well as achieving a deeper vacuum than we had on the trip strip. We will vaporize, condense, and collect our cannabinoid distillate. Similar to the last run on this machine. The terp stripped crude is pumped from the wiped film unit's heated feed tank into the top edge of the evaporator body. The spinning wipers squeegee the oil around and down the inner wall of the evaporator body and the thin film that thin film of oil is quickly heated to the new set temperature and the cannabinoids were after vaporize, just like the distilled terpenes did on the last run the THC or CBD distillate quickly condenses on the main condenser and flows down into our distillate collection vessel. The crude remaining on the evaporator body wall is wiped around and down and flows into our residue collection vessel. This 'one-pass' crude can be run again later at higher temperatures with diminishing returns. This is the end of the line for THC, but CBD distillate can be crystallized into Isolate. Delta nine THC's natural state is a light golden colored oil. So if we want THC crystals, we would have had to go after the THCA, which is crystalline in nature, before the decarb step. It is worth noting here that if we are after the THCA crystals, hydrocarbon extraction is 100% the way to go. Our CBD distillate can now be crystallized into Isolate if we want to take purification to the next level. The crystallization process starts with dissolving CBD distillate into pentane in a jacketed reactor vessel. The dissolved the CBD/pentane mix is moved into a jacketed crystallization tank and incrementally dropped in temperature over time. Once crystallization is complete, the crystals can be filtered out and collected as isolate, or re dissolved and crystallized again for an even higher purity final product.

Alright, well that takes us through the full extraction, distillation and crystallization workflow. I plan to record some more episodes on other lab related topics as the season progresses. Stay tuned for additional episodes with topics like breaking down your vacuum system, discussing lab testing, and what to think about all the Chinese equipment that's coming onto the market. Also, if you want to hear something specific, let me know. Email me my emails Jason at modern extractor.com I'll be excited to hear from you. If you guys like the show, please subscribe, the more subscribers I get the better guests I can get on in the future. Well with that, a big heartfelt thanks to everyone for tuning in to the first ever episode of the modern extractor. New episodes will be out every Tuesday. I'm Jason Showard. Let's talk soon!